Analysis of underivatizated patulin by a GC-MS technique

Journal of Food Protection

Volumn 62, Issue 2, 1999, Pages 202-205

  Llovera, Montserrat ^a   Viladrich, Remei ^a   Torres, Mercè ^a   Canela, Ramon ^a,b  

^a UNIVERSITY OF LLEIDA   (Spain)

^b Centre R+D de Lleida   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

FRUIT JUICE; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; PATULIN; SECONDARY METABOLITE;

EID: 0033083269     PISSN: 0362028X     EISSN: None     Source Type: Journal    
DOI: 10.4315/0362-028X-62.2.202     Document Type: Article

References (18)

1. Bartolomé, B, M. L. Bengochea, F. J Pérez-Ilzarbe, T. Hernandez, I. Estrella, and G. Gómez-Cordovés. 1994. Determination of patulin in apple juice by high performance liquid chromatography with diode array detection. J. Chromatogr. 664:39-43.
2. Brause, A. R., M. W. Truckesess, F. S. Thomas, and S. W. Page. 1996. Determination of patulin in apple juice by liquid chromatography: collaborative study. J. Assoc. Off. Anal. Chem. 79:451-455.
3. Budavari, S., ed. 1996. The Merck index, 12th ed. Merck & Co., Whitehouse Station, N.J.
4. Doherty, L. 1992. Improving the sensitivity of your GC/MS system with electronic pressure control. Hewlett-Packard Company, MS application brief MS 92-5, 23, 5091-5493E.
5. FAO. 1996. Worldwide regulations for mycotoxins. Food and nutrition paper, advance copy. FAO, Rome.
6. Fujimoto, Y., T. Suzuki, and Y. Hoshino. 1975. Determination of penicillic acid and patulin by gas-liquid chromatography with an electron-capture detector. J. Chromatogr. 105:99-106.
7. IARC. 1986. IARC Monographs on the evaluation of the carcinogenic risk of chemicals to humans, vol 40. Some naturally occurring and synthetic food components, furocoumarins and ultraviolet radiation. International Agency for Research on Cancer, Lyon.
8. Jefferys, E. G. 1952. The stability of antibiotics in soils. J. Gen. Microbiol. 7:295.
9. Kubacki, S. J., and H. Goszcz. 1988. HPLC methods for the determination of patulin in apple juice. Pure Appl. Chem. 60:871-876.
10. Lovett, J., and J. T. Peeler. 1973. Effect of pH on the thermal destruction kinetics of patulin in aqueous solution. J. Food Sci. 38: 1094-1095.
11. Price, K. R. 1979. A comparison of two quantitative mass spectrometric methods for the analysis of patulin in apple juice. Biomed. Mass Spectrom. 6:573-574.
12. Priest, J. W., and R. J. Light. 1990. Applications of high performance liquid chromatography to quantitation of metabolites and enzymes of the patulin pathway from Penicillium patulum. J. Chromatogr. 513:237-246.
13. Rovira, R., F. Rivera, V. Sanchis, and R. Canela. 1993. Improvements in the quantitation of patulin in apple juice by high performance liquid chromatography. J. Agric. Food Chem. 41:214-216.
14. Scott, P. M. 1974. Collaborative study of a chromatographic method for determination of patulin in apple juice. J. Assoc. Off. Anal. Chem. 57:621-625.
15. Scott, P. M., and B. P. C. Kennedy. 1973. Improved method for the thin layer chromatographic determination of patulin in apple juice. J. Assoc. Off. Anal. Chem. 56:813-816.
16. Suzuki, T., Y. Fujimoto, Y. Hoshino, and A. Tanaka. 1975. Trimethylsilylation of penicillic acid and patulin, and the stability of the products. J. Chromatogr. 105:95-98.
17. Tarter, E. J., and P. M. Scott. 1991. Determination of patulin by capillary gas chromatography of the heptafluorobutyrate derivative. J. Chromatogr. 538:441-446.
18. Van Egmond, H. P. 1989. Current situation on regulations for mycotoxins. Overview of tolerances and status of standard methods of sampling and analysis. Food Addit. Contam. 6:139-188.