Measuring induction period for calcium sulfate dihydrate precipitation

AIChE Journal

Volumn 45, Issue 2, 1999, Pages 390-397

  Lancia, Amedeo ^a   Musmarra, Dino ^b   Prisciandaro, Marina ^c  

^a UNIVERSITY OF NAPLES FEDERICO II   (Italy)

^b CNR   (Italy)

^c UNIVERSITY OF L'AQUILA   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

CRYSTALLIZATION; CRYSTALLIZERS; HELIUM NEON LASERS; HYDRATES; LIGHT SCATTERING; LIGHT TRANSMISSION; PRECIPITATION (CHEMICAL); REACTION KINETICS; SUPERSATURATION; SURFACE TENSION; THERMAL EFFECTS;

BATCH CRYSTALLIZERS; CALCIUM SULFATE DIHYDRATE; OPTICAL DIAGNOSTICS;

GYPSUM;

CALCIUM SULFATE;

ARTICLE; CHEMICAL ANALYSIS; CRYSTALLIZATION; LASER; PRECIPITATION; TEMPERATURE;

EID: 0033082374     PISSN: 00011541     EISSN: None     Source Type: Journal    
DOI: 10.1002/aic.690450218     Document Type: Article

References (20)

1. Amathieu, L., and Boistelle, R., "Crystallization Kinetics of Gypsum from Dense Suspension of Hemihydrate in Water," J. Cryst. Growth, 88, 183 (1988).
2. 4 Solubility in Multicomponent Aqueous Solutions," Chem. Eng. J., 24, 191 (1982).
3. Bromley, L. A., "Thermodynamic Properties of Strong Electrolytes in Aqueous Solutions," AIChE J., 19, 313 (1973).
4. Budz, J., A. G. Jones, and J. W. Mullin, "Effect of Selected Impurities on the Continuous Precipitation of Calcium Sulphate (Gypsum)," J. Chem. Tech. Biotechnol., 36, 153 (1986).
5. He, S., J. E. Oddo, and M. B. Tomson, "The Nucleation Kinetics of Calcium Sulfate Dihydrate in NaCl Solutions up to 6 m and 90°C," J. Coll. Int. Sci., 162, 297 (1994).
6. Liu, S. T., and G. H. Nancollas, "A Kinetic and Morphological Study of the Seeded Growth of Calcium Sulfate Dihydrate in the Presence of Additives," J. Coll. Int. Sci., 52, 593 (1975).
7. Marshall, W. L., and R. Slusher, "Thermodynamics of Calcium Sulfate Dihydrate in Aqueous Sodium Chloride Solutions, 0-110°," J. Phys. Chem., 70, 4015 (1966).
8. Mullin, J. W., Crystallization, 3rd ed., Butterworth-Heinemann Ltd., Oxford (1993).
9. Nielsen, A. E., Kinetics of Precipitation, Pergamon Press, Oxford (1964).
10. Packter, A., "Precipitation of Sparingly Soluble Alkane-Earth Metal and Lead Salts: Nucleation and Growth Orders During the Induction Period," J. Chem. Soc., 859 (1968).
11. Packter, A., "The Precipitation of Calcium Sulphate Dihydrate from Aqueous Solution-Induction Period, Crystal Numbers and Final Size," J. Cryst. Growth, 21, 191 (1974).
12. Prisciandaro, M., "Cristallizzazione del Solfato di Calcic Biidrato nel Processo di Desolforazione ad Umido dei Fumi Delia Combustione," PhD Diss., Univ. of Naples "Federico II," Italy (1998).
13. Rasmussen, D. H., and A. P. MacKenzie, "Clustering in Supercooled Water," J. Chem. Phys., 59, 5003 (1973).
14. Ratinov, V. B., and O. M. Todes, Dokl. Akad. Nauk SSSR, 132, 402 (1960).
15. Sarig, S., and J. W. Mullin, "Effect of Impurities on Calcium Sulphate Precipitation," J. Chem. Tech. Biotechnol., 32, 525 (1982).
16. Söhnel, O., "Electrolyte Crystal-Aqueous Solution Interfacial Tensions from Crystallization Data," J. Crystal Growth, 57, 101 (1982).
17. Söhnel, O., and J. Garside, Precipitation, Butterworth-Heinemann Ltd., Oxford (1992).
18. Söhnel, O., and J. W. Mullin, "A Method for the Determination of Precipitation Induction Periods," J. Crystal Growth, 44, 377 (1978).
19. Söhnel, O., and J. W. Mullin, "Interpretation of Crystallization Induction Periods," J. Coll. Int. Sci., 123, 43 (1988).
20. Wood, G. R., and A. G. Walton, "Homogeneous Nucleation Kinetics of Ice from Water," J. Appl. Phys., 41, 3027 (1970).