Determination of bis(tributyltin) oxide by GC-MS with on-line hydride derivatization: Application to drug substance analysis

Journal of Pharmaceutical and Biomedical Analysis

Volumn 19, Issue 3-4, 1999, Pages 327-333

  O'Brien, Thomas P ^a   Dowling, Thomas M ^a   Moeder, Charles W ^a   Bicker, Gary R ^a  

^a MERCK RESEARCH LABORATORIES   (United States)

Author keywords

Determination of bis(tributyltin) oxide; GC MS determination of tributyltin; On line hydride derivatization; Selective ion monitoring; Tributyltin chloride; Tributyltin hydride

Indexed keywords

BIS(TRIBUTYLTIN) OXIDE; DRUG; SODIUM BOROHYDRIDE; TRIBUTYLTIN; TRIBUTYLTIN HYDRIDE; UNCLASSIFIED DRUG;

ARTICLE; DERIVATIZATION; DEVICE; DRUG CONTAMINATION; DRUG DETERMINATION; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; PRIORITY JOURNAL;

BOROHYDRIDES; DRUG CONTAMINATION; EVALUATION STUDIES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; MAXIMUM ALLOWABLE CONCENTRATION; ORGANOTIN COMPOUNDS; PHARMACEUTICAL PREPARATIONS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; TRIALKYLTIN COMPOUNDS;

EID: 0033047212     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0731-7085(98)00125-3     Document Type: Article

References (24)

1. Dowling T.M., Uden P.C. J. Chromatogr. 644:1993;153-160.
2. Neumann W.P. Synthesis. 8:1987;665-683.
3. Milstein D., Silke J.K. J. Am. Chem. Soc. 101:1979;4992-4998.
4. Trost B.M., Keinan E. Tetrahedron Lett. 21:1980;2595-2598.
5. Dyne D., Chana B.S., Smith N.J., Crocker J. Anal. Chim. Acta. 246:1991;351-357.
6. Lattard C., Rocca J.L. Analysis. 11(9):1983;457-462.
7. Schulze G., Lehmann C. Anal. Chim. Acta. 288(3):1994;215-220.
8. Rivas C., Ebdon L., Hill S.J. Quim. Anal. 14(3):1995;142-147.
9. Compano R., Granados M., Leal C., Prat M.D. Anal. Chim. Acta. 314(3):1995;175-182.
10. Hansen D.R., Lillie C.H., Hill H.H. J. Chromatogr. Sci. 23(5):1985;208-213.
11. Hansen D.R., Gilfoil T.J., Hill H.H. Anal. Chem. 53(6):1981;857-861.
12. Sasaki K., Ishizaka T., Suzuki T., Takashi S., Saito Y. Anal. Chem. 71(2):1988;360-363.
13. Takeuchi M., Mizuishi K., Yamanobe H., Watanabe Y. Bunseki Kagaku. 36(3):1987;138-142.
14. Mishima M., Maruyama T., Kohiyama M., Murakami C., Kumagaya M., Sumiyashi M., Asahi T., Nozawa T., Tanaka Y., Ogawa A., Matsuzuki N., Nanpo T., Ono K., Takahashi M., Ito K. Bunseki Kagaku. 33(8):1984;57-60.
15. Aue W.A., Flinn B.J., Flinn C.G., Paramasigamani V., Russell K.A. Can. J. Chem. 67:1988;402-410.
16. Meinema H.A., Burger-Wiersma T., Versluis-de Haan G., Gevers E.C. Environ. Sci. Technol. 12(3):1978;288-293.
17. Caricchia A.M., Chiavarini S., Cremisini C., Morabito R., Ubaldi C. Int. J. Environ. Anal. Chem. 53(1):1993;37-52.
18. Astruc M., Pinel R., Astruc A. Mikrochim. Acta. 109:1992;73-77.
19. Cai Y., Rapsomanikis S., Andreae M.O. Anal. Chim. Acta. 274(2):1993;243-251.
20. Rodriguez Pereiro I., Schmitt V.O., Szpunar J., Donard O.F.X., Lobinski R. Anal. Chem. 68:1996;4135-4140.
21. Shushunova A.F., Kutsovskaya V.V., Skovorodina M.V., Makin G.I. Zh. Anal. Khim. 44(4):1989;745-748.
22. Craig P.J., Clark S. Analyst. 112:1987;1781-1782.
23. R.L. Smith, EPA Region III Risk-Based Concentration Table, Third Quarter 1994.
24. Kacprzak J.L. Int. J. Environ. Anal. Chem. 38(4):1990;561-564.