Iodine and its interhalogen compounds: Versatile reagents in carbohydrate chemistry IX. A mild and selective deprotection of tert-butyldimethylsilyl (TBDMS) ethers in the presence of various protecting groups using iodine monobromide

Synlett

Volumn , Issue 3, 1999, Pages 311-312

  Kartha, K P Ravindranathan ^a   Field, Robert A ^a  

^a UNIVERSITY OF ST ANDREWS   (United Kingdom)

Author keywords

Iodine monobromide; TBDMS ethers

Indexed keywords

BROMINE DERIVATIVE; ETHER DERIVATIVE; IODINE DERIVATIVE;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL REACTION; CHEMICAL STRUCTURE;

EID: 0033020247     PISSN: 09365214     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (6)

1. For Part VIII see Kartha, K.P.R.; Field, R.A. Carbohydr. Lett. 1998, 3, 179.
2. 5
3. Vaino, A.R.; Szarek, W.A. Chem. Commun. 1996, 2351 and references 2, 4 and 8-19 sited therein.
4. Szarek, W.A.; Zamojski, A.; Tiwari, K.N.; Ison, E.R. Tetrahedron Lett. 1986, 27, 3827.
5. Kartha, K.P.R.; Field, R.A. Tetrahedron Lett., 1996, 38, 8233.
6. 5, which eluted first, was obtained in ≤5% yield followed by (2) in 85-90% yield.