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Volumn 29, Issue 3, 1999, Pages 409-413

A short and convenient preparation of (E)-3-(1-cyclohexenyl)-2- propenoic acid using a palladium(II) complex-catalyzed olefination

Author keywords

[No Author keywords available]

Indexed keywords

3 (1 CYCLOHEXENYL) 2 PROPENOIC ACID; ALKALOID DERIVATIVE; ALKENE; CYCLOHEXANONE; HIMBACINE; PALLADIUM COMPLEX; UNCLASSIFIED DRUG;

EID: 0032986384     PISSN: 00397911     EISSN: None     Source Type: Journal    
DOI: 10.1080/00397919908085782     Document Type: Article
Times cited : (3)

References (27)
  • 17
    • 85038205553 scopus 로고    scopus 로고
    • note
    • 1H NMR analysis.
  • 18
    • 85038199279 scopus 로고    scopus 로고
    • note
    • The price of 2,6-di-tert-butyl-4-methylpyridine (Aldrich): $273.65 per 25g.
  • 20
    • 0345539025 scopus 로고
    • 1-Bromocyclohexene was supplied from Allied-Signal, Inc., Morristown, New Jersey 07962. For its preparation, see: (a) Bandodakar, B. S.; Nagendrappa, G. Synthesis 1990, 843.
    • (1990) Synthesis , pp. 843
    • Bandodakar, B.S.1    Nagendrappa, G.2
  • 21
    • 0342278755 scopus 로고
    • (b) Ndebeka, G.; Raynal, S.; Caubere, P. J. Org. Chem. 1980, 45, 5394. For its Heck reaction with methyl acrylate, see: Kim, J. I. Taehan Hwahakhoe Chi 1983, 27, 441; CA 1984, 100, 156199.
    • (1980) J. Org. Chem. , vol.45 , pp. 5394
    • Ndebeka, G.1    Raynal, S.2    Caubere, P.3
  • 22
    • 6544253148 scopus 로고
    • (b) Ndebeka, G.; Raynal, S.; Caubere, P. J. Org. Chem. 1980, 45, 5394. For its Heck reaction with methyl acrylate, see: Kim, J. I. Taehan Hwahakhoe Chi 1983, 27, 441; CA 1984, 100, 156199.
    • (1983) Taehan Hwahakhoe Chi , vol.27 , pp. 441
    • Kim, J.I.1
  • 23
    • 6544255419 scopus 로고
    • (b) Ndebeka, G.; Raynal, S.; Caubere, P. J. Org. Chem. 1980, 45, 5394. For its Heck reaction with methyl acrylate, see: Kim, J. I. Taehan Hwahakhoe Chi 1983, 27, 441; CA 1984, 100, 156199.
    • (1984) CA , vol.100 , pp. 156199
  • 24
    • 0027416248 scopus 로고
    • 1-Iodocyclohexene was prepared in two steps from cyclohexanone via the corresponding vinyl phosphate. See: Lee, K.; Wiemer, D. Tetrahedron Lett. 1993, 54, 2433.
    • (1993) Tetrahedron Lett. , vol.54 , pp. 2433
    • Lee, K.1    Wiemer, D.2
  • 25
    • 85038206178 scopus 로고    scopus 로고
    • note
    • 1H NMR analysis showed that there existed 12-25% of the byproduct methyl cinnamate in the reaction mixture in all the experiments.
  • 26
    • 85038196151 scopus 로고    scopus 로고
    • note
    • 2O (40:60); flow rate, 1.5 mL/min; detector, 230 nm; room temperature.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.