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17
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85038205553
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note
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1H NMR analysis.
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18
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85038199279
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note
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The price of 2,6-di-tert-butyl-4-methylpyridine (Aldrich): $273.65 per 25g.
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19
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0000202518
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Scott, W. J.; Pena, M. R.; Sward, K.; Stoessel, S. J.; Stille, J. K. J. Org. Chem. 1985, 50, 2302.
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20
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0345539025
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1-Bromocyclohexene was supplied from Allied-Signal, Inc., Morristown, New Jersey 07962. For its preparation, see: (a) Bandodakar, B. S.; Nagendrappa, G. Synthesis 1990, 843.
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Synthesis
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Bandodakar, B.S.1
Nagendrappa, G.2
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21
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0342278755
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(b) Ndebeka, G.; Raynal, S.; Caubere, P. J. Org. Chem. 1980, 45, 5394. For its Heck reaction with methyl acrylate, see: Kim, J. I. Taehan Hwahakhoe Chi 1983, 27, 441; CA 1984, 100, 156199.
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Ndebeka, G.1
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Caubere, P.3
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22
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6544253148
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(b) Ndebeka, G.; Raynal, S.; Caubere, P. J. Org. Chem. 1980, 45, 5394. For its Heck reaction with methyl acrylate, see: Kim, J. I. Taehan Hwahakhoe Chi 1983, 27, 441; CA 1984, 100, 156199.
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Taehan Hwahakhoe Chi
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Kim, J.I.1
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23
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6544255419
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(b) Ndebeka, G.; Raynal, S.; Caubere, P. J. Org. Chem. 1980, 45, 5394. For its Heck reaction with methyl acrylate, see: Kim, J. I. Taehan Hwahakhoe Chi 1983, 27, 441; CA 1984, 100, 156199.
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CA
, vol.100
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24
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0027416248
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1-Iodocyclohexene was prepared in two steps from cyclohexanone via the corresponding vinyl phosphate. See: Lee, K.; Wiemer, D. Tetrahedron Lett. 1993, 54, 2433.
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Lee, K.1
Wiemer, D.2
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25
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85038206178
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note
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1H NMR analysis showed that there existed 12-25% of the byproduct methyl cinnamate in the reaction mixture in all the experiments.
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26
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85038196151
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note
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2O (40:60); flow rate, 1.5 mL/min; detector, 230 nm; room temperature.
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