Chemistry of N-heterocyclic compounds: Part I: Regioselective synthesis of macrocycles containing 4-amino-1,2,4-triazoles

Synthetic Communications

Volumn 29, Issue 10, 1999, Pages 1711-1717

  Chande, Madhukar S ^a   Athalye, Shailesh S ^a  

^a INSTITUTE OF SCIENCE   (India)

Author keywords

[No Author keywords available]

Indexed keywords

4 AMINO 1,2,4 TRIAZOLE; 4 AMINO 3,5 DIMERCAPTOTRIAZOLE; ALKANE DERIVATIVE; MACROCYCLIC COMPOUND; TRIAZOLE DERIVATIVE; UNCLASSIFIED DRUG;

ALKYLATION; ARTICLE; CHEMICAL STRUCTURE; REACTION ANALYSIS; STEREOCHEMISTRY; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 0032972668     PISSN: 00397911     EISSN: None     Source Type: Journal    
DOI: 10.1080/00397919908086158     Document Type: Article

References (9)

1. Newkome, G.R ; Sauere, J.D ; Roper, J.M. ; Hager, D.C ; Chemical Reviews, 1977, 77, 513-517.
2. Gokel, G.W ; " Crown Ethers and Cryptands ", University of Miami , Coral Gables, Florida, U.S.A. The Royal Society of Chemistry, 1991, pp 49-52
3. a) Sinha, B.K ; Singh, R ; Srivastava, J.P & Mishra, L.K., J inorg.nucl.Chem., 1977, 39, 1797-1801.
4. b) Sandstrom .J, Acta Chem Scand, 1961, 15, 1295.
5. Guha, P.C. & De, S.C., J Chem Soc., 1924, 125, 1215.
6. +, m/z 376 (6%). Elemental Analysis [(cal)/obs] : C( 31.91%)/31.87%, H (425%) / 4.21%, N (29.78%) / 29.69%, S (34.04%) / (34.00).
7. 2-S-), 154.765(C=N ), 172.750 (C=S) ppm Elemental Analysis [(cal)/obs] : C (22.36%) / 22.28%, H (3.10%) / 3.01% , N (34.78%) / 34.66%, S (39.75%)/39.71%.
8. + : m/z 362 ( 1%). Elemental Analysis [(cal)/obs] : C (29.83%) / 29.72%, H (3 86%) / 3.81% , N (30.93%) / 30.80%, S (35.35%) / 35.21%.
9. + : m/z 348 (52%). Elemental Analysis [(cal)/obs] : C (27.58%) / 27.51%, H (3.44%) / 3.39%, N (32.18%) / 32.11%, S (36.76%) / 36.67 %.