Facile methods for the direct conversions of aryl acetates into the corresponding methoxymethyl ethers or silyl ethers

Synthetic Communications

Volumn 29, Issue 13, 1999, Pages 2217-2223

  Oriyama, Takeshi ^a   Noda, Kojiro ^a   Sugawara, Satomi ^a  

^a IBARAKI UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

ARYL ACETATE; METHOXYMETHYL ETHER; SILANE DERIVATIVE; UNCLASSIFIED DRUG;

ANALYTIC METHOD; ARTICLE; BINDING KINETICS; CHEMICAL REACTION KINETICS; HYDROXYLATION; REACTION ANALYSIS; SYNTHESIS;

EID: 0032916056     PISSN: 00397911     EISSN: None     Source Type: Journal    
DOI: 10.1080/00397919908086220     Document Type: Article

References (9)

1. (a) Greene, T. W., and Wuts, P. G. M. "Protective Groups in Organic Synthesis" 2nd Ed., John Wiley & Sons, New York, 1991.
2. (b) Kocienski, P. J. "Protecting Groups" Georg Thieme Verlag, New York, 1994.
3. (a) Oriyama, T., Kimura, M., Oda, M., and Koga, G. Synlett, 1993, 437.
4. (b) Oriyama, T., Kimura, M., and Koga, G. Bull. Chem. Soc. Jpn., 1994, 67, 885.
5. (c) Oriyama, T., Oda, M., Gono, J., and Koga, G. Tetrahedron Lett., 1994, 35, 2027.
6. (d) Oriyama, T., Yatabe, K., Kawada, Y., and Koga, G. Synlett, 1995, 45.
7. (e) Oriyama, T., Yatabe, K., Sugawara, S., Machiguchi, Y., and Koga, G. Synlett, 1996, 523.
8. Oriyama, T., Noda, K., and Yatabe, K. Synlett, 1997, 701.
9. 2O and the combined extracts were washed with brine, dried over anhydrous sodium sulfate, filtered, and concentrated in vacuo. The crude product was purified by thin-layer chromatography on silica gel to give 1-t-butyldimethylsilyloxy-4-methylbenzene (79.6 mg, 93%).