Inexpensive protocol for reduction of imines to amines using polymethylhydrosiloxane (PMHS)

Synthetic Communications

Volumn 29, Issue 22, 1999, Pages 3981-3987

  Chandrasekhar, S ^a   Reddy, M Venkat ^a   Chandraiah, L ^a  

^a INDIAN INSTITUTE OF CHEMICAL TECHNOLOGY   (India)

Author keywords

[No Author keywords available]

Indexed keywords

AMINE; IMINE; SILOXANE; ZINC CHLORIDE;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; REDUCTION; SYNTHESIS;

EID: 0032873376     PISSN: 00397911     EISSN: None     Source Type: Journal    
DOI: 10.1080/00397919908085918     Document Type: Article

References (16)

1. MDL Drug Data Report, MDL information systems, Inc., Sanleandro., CA.
2. Larock, R.C. Comprehensive Organic Transformations, 1988, 421-430.
3. a. Kimpe, N.D.; Stanoeva, E.; Verhe, R. and Schamp, N. Synthesis, 1988, 587.
4. b. Itsuno, S.; Sakurai, Y. and Ito, K. Synthesis, 1988, 995.
5. c. Periasamy, M.; Devasagayaraj, A.; Sathyanarayana, N. and Narayana, C. Synth. Commun., 1989, 19, 565.
6. a. Billman, J.H. and Tai, K.M. J. Org. Chem 1958, 535
7. b. Cherest, M.; Felkin, H. and Prudent, N. Tetrahedron Lett., 1968, 2199.
8. Billman, J. H. and McDowell, J. W. J. Org. Chem. 1961, 1437.
9. a. Ojima, I.; Kogure, T. and Nagai, Y. Tetrahedron Lett., 1973, 2475.
10. b. Langloss, N.; Dang, T. P. and Kagan, H.B. Tetrahedron Lett., 1973, 4865.
11. c. Lopez, R.M. and Fu, G.C. Tetrahedron 1997, 53, 16349.
12. a. Beeker, H.; Brunner, H.; Mahboobi, S. and Wiegrebe, W. Angew Chem. Int.Ed., 1987, 97, 969.
13. b. Kagan, H.B.; Langlois, N. and Dang, J.P. J. Organomet. Chem., 1975, 90,
14. c. Andrianov, K.A.; Filimonua, M.I. and Sidorov, V.I. J. Organomet. Chem., 1977, 142, 31.
15. Vardaguer, X.; Lange, U.E.W. and Buehwald, S.L. Angew. Chem. Int. Ed. 1998, 37(8), 1103.
16. 2 activated PMHS for the reduction of carbonyl compounds, see Chandrasekhar, S.; Ravindra Reddy, Y. and Rama Rao C. Synth. Commun., 1997, 27, 2251.