Identification of an intact sydnonimine ring depending on the reaction substituents of mesocarb by gas chromatography/mass spectrometry

Journal of Mass Spectrometry

Volumn 34, Issue 10, 1999, Pages 1079-1086

  Lee, JeongAe ^a   Jeung, Hyeonsook ^a   Kim, Keon ^b   Lho, Dong Seok ^a  

^a Korea Institute of Science and Technology   (South Korea)

^b Korea University   (South Korea)

Author keywords

Intact sydnonimine ring; Mesocarb intermediate; Methylated N nitroso N cyanomethylamphetamine; Pyrolysis; Trifluoroacylated sydnophen; Trimethylsilylated sydnophen

Indexed keywords

CHEMICAL COMPOUND; KETENE DERIVATIVE; METHYL GROUP; NITROGEN; SYDNOCARB; SYDNOFEN; TRIMETHYLSILYL DERIVATIVE;

ARTICLE; CHEMICAL MODIFICATION; CHEMICAL REACTION; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; METHYLATION; PRIORITY JOURNAL; PYROLYSIS;

EID: 0032863197     PISSN: 10765174     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1096-9888(199910)34:10<1079::AID-JMS869>3.0.CO;2-M     Document Type: Article

References (19)

1. Sandor L, Erado SL, Kiss B, Rosdy B. J. Pharmacol. Pharm. 1981; 33: 141.
2. Hund P, Raynaud J, Laven M, Schacht U. Biochem. Pharmacol. 1979; 28: 2011.
3. Prokudin WN. Gesundheitswesen 1977; 32: 805.
4. Tamas J, Polgar M, Czira G, Vereczkey L. Recent Dev. Mass Spectrom. Biochem. Med. 1979; 2: 43.
5. Polgar M, Vereczkey L, Szporny L, Czrra G, Tamas J, Gacs-Baitz E, Holly S. Xenobiotica 1979; 9: 511.
6. Thieme D, Grosse J, Lang R, Muller RK. In Recent Advances in Doping Analysis, Proceedings of the Cologne Workshop on Dope Analysis, 12th, 1994. Donike M (ed). Sport und Buch Strauss: Cologne, 1995; 275.
7. Ventura R, Nadal T, Alcalde P, Segura J. J. Chromatogr. 1993; 647: 203.
8. Yang S, Zhu S, Yang Z. In Recent Advances in Doping Analysis, Proceedings of the Cologne Workshop on Dope Analysis, 14th, 1996. Schaenzer W (ed). Sport und Buch Strauss: Cologne, 1997; 377.
9. Altshuler RA, Kovalenko TA, Holodov LE, Plievkton MK. Khim. Farm. Zh. 1976; 10: 20.
10. Ollis WD, Ramsden CA. In Advances in Heterocyclic Chemistry, vol. 19. Katritzky AR, Boulton AJ (ed). Academic Press: New York, 1976; 3.
11. Pyo H, Park S, Park J, Yoo JK, Yoon B. J.Chromatogr. 1996; 687: 261.
12. Potts KT, Armbruster R, Houghton E, Kane J. Org. Mass Spectrom. 1972; 7: 203.
13. Undheim K, El-Gendy MAF, Hurum T. Org. Mass Spectrom. 1974; 9: 1242.
14. de Boer D, van Ooijen RD, Maes RAA. In Recent Advances in Doping Analysis, Proceedings of the Cologne Workshop Dope Analysis, 12th, 1994, Donike M (ed). Sport und Buch Strauss: Cologne, 1995; 305.
15. Daeniker HU, Druey J. Helv. Chim. Acta 1962; 45: 2441.
16. Kholodov LE, Yashunskii VG. Khim. Geterotsikl. Soedin. Akad. Nauk. Latv. SSR 1965; 328; Chem. Abstr. 1965; 63: 14652.
17. Kholodov LE, Yashunskii VG. Khim. Geterotsikl. Soedin. Akad. Nauk. Latv. SSR 1965; 328; Chem. Abstr. 1965; 63: 14652.
18. Goudie RS, Preston PN, Palmer MH. Org. Mass Spectrom. 1969; 2: 953.
19. Dougherty RC, Foltz RL, Kier LB. Tetrahedron 1989; 26: 1970.