Spectrophotometric determination of dipyrone in pharmaceutical preparations by using chromotropic acid

Farmaco

Volumn 54, Issue 9, 1999, Pages 629-635

  Sakiara, Kelly Alessandra ^a   Pezza, Leonardo ^a   Bladimiros Melios, Cristo ^a   Redigolo Pezza, Helena ^a   De Moraes, Mercedes ^a  

^a SÃO PAULO STATE UNIVERSITY UNESP   (Brazil)

Author keywords

Chromotropic acid; Dipyrone; Pharmaceutical preparations; Spectrophotometric determination

Indexed keywords

DIPYRONE; DRUG; FORMALDEHYDE; SULFURIC ACID;

ARTICLE; COLOR; CONTROLLED STUDY; DRUG ANALYSIS; DRUG DETERMINATION; MEASUREMENT; NONHUMAN; OXIDATION; SPECTROPHOTOMETRY; TECHNIQUE;

EID: 0032863173     PISSN: 0014827X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0014-827X(99)00073-7     Document Type: Article

References (65)

1. Srivastava M.K., Ahmad S., Singh D., Shukla I.S. Tritimetric determination of dipyrone and paracetamol with potassium hexacyanoferrate(III) in an acidic medium. Analyst. 110:1985;735-737.
2. Brazilian Pharmacopoeia, third ed., Organização Andrei Editora SA, São Paulo, Brazil, 1977, p. 408.
3. Inandar M.C., Sanghavi N.M. Estimation of analgin in dosage forms by titration with perchloric acid. Indian J. Pharm. 33(5):1971;94-95.
4. Murata T., Ochiai T. Application of nonaqueous titration of drugs. Kumamoto Pharm. Bull. 4:1959;15-17.
5. Costa N., Ksenija V., Mirjana N. Coulometric determination of some analgesic pyrazolone derivations in pharmaceutical formulations. Acta Pharm. Jugosl. 34:1984;177-182.
6. Roushdi I.M., Soliman S.A., Sadek M.H. Polarographic determination of sodium phenyl dimethylpyrazolone methylaminomethanesulfonate in pharmaceutical preparations. J. Pharm. Sci. (UAR). 13:1971;347-352.
7. E.Y. Fatova, N.S. Evtushenko, I.V. Pakhomova, Simultaneous determination of analgin, amidopyrine, phenobarbital, codeine and caffeine in Pentalgin tablets by thin-layer chromatography and spectrophotometric densitometry, Farmatsiya (Moscow) 40 (6) (1991) 31-35 [Chem. Abstr. 116 (1992) 28300k].
8. E.Y. Fatova, N.S. Evtushenko, I.V. Pakhomova, Simultaneous determination of analgin, amidopyrine, phenobarbital, codeine and caffeine in Pentalgin tablets by thin-layer chromatography and spectrophotometric densitometry, Farmatsiya (Moscow) 40 (6) (1991) 31-35 [Chem. Abstr. 116 (1992) 28300k].
9. Eddine N.H., Bressolle F., Mandrou B., Fabre H. Stability indicating assay for dipyrone. 2. Separation and quantitative determination of dypirone and its degradation products by high performance liquid chromatography. Analyst. 107:1982;67-70.
10. Uno T., Yamamoto M. Fluorimetric determination of sulpyrine with quinonedichlorodiimide. Jpn. Anal. 22:1973;1420-1423.
11. Chatterjee P.K., Jain C.L., Sethi P.D. Simultaneous spectrophotometric determination of oxyphenbutazone and analgin in pharmaceutical formulations. Indian J. Pharm. Sci. 49:1987;111-113.
12. Bagavant G., Rowhani V. Ultraviolet spectrophotometric analysis of binary mixtures of analgin-paracetamol and analgin-oxyphenbutazone. Indian Drugs. 23(6):1986;373-375.
13. Abdine H., El-Sayed M.A.E., Abdel-Hamed M. Spectrophotometric determination of dipyrone in combination with quinine. Acta Pharm. Jugosl. 28:1978;75-81.
14. V.G. Belikov, S.K. Matsueva, Determination of analgin by a differential spectrophotometric method, Khim. Farm. Zh. 3 (6) (1969) 44-46 [Chem. Abstr. 71 (1969) 74091t].
15. V.G. Belikov, S.K. Matsueva, Determination of analgin by a differential spectrophotometric method, Khim. Farm. Zh. 3 (6) (1969) 44-46 [Chem. Abstr. 71 (1969) 74091t].
16. L. Varcel, Spectrophotometric determination of noramidopyrine methanesulfonate sodium in analgin Spofa veterinary injections, Cesk. Farm. 16 (9) (1967) 494-495 [Chem. Abstr. 68 (1968) 81453d].
17. L. Varcel, Spectrophotometric determination of noramidopyrine methanesulfonate sodium in analgin Spofa veterinary injections, Cesk. Farm. 16 (9) (1967) 494-495 [Chem. Abstr. 68 (1968) 81453d].
18. Marciniec B., Wojeiechowska B. Determination of 5-pyrazolinone derivatives in pharmaceutical preparations. I. Spectrophotometric determination of two-component preparations containing propyphenazone. Acta Pol. Pharm. 46:1989;248-257.
19. Bozdogan A., Acar A.M., Kunt G., Caglar H. Simultaneous determination of paracetamol, metamizol sodium and caffeine in tablet preparations by partial least-squares spectrophotometric calibration. Pharmazie. 49:1994;457-458.
20. Erk N., Onur F. Simultaneous determination of analgine and paracetamol in tablets by spectrophotometric methods. Anal. Lett. 30:1997;1201-1210.
21. El-Sadek M., Salem H., Khier A.B. First derivative spectrophotometric method for determination of ascorbic acid and analgin in combination. Spectrosc. Lett. 23:1990;77-86.
22. El-Zeany A., Moustafa A.A., Abdelkawy M., Abdelghany M.F. Simultaneous determination of papaverine hydrochloride/analgin mixture in presence of homatropine methyl bromide in pharmaceutical preparations. Bull. Fac. Pharm. (Cairo Univ.). 31(2):1993;141-146.
23. Erk N., Onur F. Spectrophotometric simultaneous determination of analgin and hyoscine N-butyl bromide in sugar-coated tablets. Anal. Lett. 29:1996;369-380.
24. S.K. Matsueva, E.N. Vergeichik, V.G. Belikov, Use of a second spectral derivative for determining 5-pyrazolone derivatives, Metody Anal. Kontrol. Kach. Prod. Khim. Promsti 5 (1978) 20-22 [Chem. Abstr. 89 (1978) 204296y].
25. S.K. Matsueva, E.N. Vergeichik, V.G. Belikov, Use of a second spectral derivative for determining 5-pyrazolone derivatives, Metody Anal. Kontrol. Kach. Prod. Khim. Promsti 5 (1978) 20-22 [Chem. Abstr. 89 (1978) 204296y].
26. Vasileva-Alexandrova P. Spectrophotometric determination of analgin with monozolium and ditetrazolium salts. Mikrochim. Acta. 2(3-4):1976;247-252.
27. Qureshi S.Z., Saeed A., Haque S. Some observations on a simple method for the determination of novalgin in drug formulations with iron(III)-1,10-phenantroline. Microchem. J. 41:1990;362-365.
28. 3+/1,10-phenantroline system. Chem. Anal. Warsaw. 29(4):1984;483-489.
29. Buhl F., Hachula U. Spectrophotometric determination of antipyrine, pyramidon and novalgin by using the cerium(III)-arsenazo(III) reaction. Chem. Anal. (Warsaw). 26:1981;395-400.
30. C.S.P. Sastry, A.R. Rao, Spectrophotometric determination of some analgesic acid and anti-inflammatory agents with 3-methyl-2-benzothiazoline hydrazone hydrochloride, Mikrochim. Acta (1989) 237-244.
31. Sergeev G.M., Dorofeeva I.V., Stepanova L.G. Extraction-photometric determination of pharmaceuticals by using redox reactions. Zh. Anal. Khim. 41:1986;1694-1697.
32. Vasxileva-Alexandrova P., Shishmanov P.S. Spectrophotometric determination of dipyrone with neotetrazolium chloride. Anal. Chem. 47:1975;1432-1435.
33. P. Vasileva-Aleksandrova, Mechanism of the analgin, tetrazolium salt reaction. 1. Separation of the products of the alkaline hydrolysis of analgin. 2. Isolation of the products of analgin, Nauchni Tr. Plovdivski Univ. 19 (3) (1982) 51-61, 63-69 and Refs. therein.
34. Quereshi S.Z., Saeed H., Tausiful H. Spectrophotometric determination of novalgin in tablets by use of potassium iodate. Talanta. 36:1989;869-871.
35. Philip G. Colorimetric determination of analgin in pharmaceutical preparations. Indian J. Pharm. 36:1974;14-15.
36. F.M. Shemyakin, O.A. Ofremenko, N.A. Ovesnova, Basic dyes as reagents for drugs of an acidic nature, Farmatsiya (Moscow) 26 (1) (1977) 39-42 [Chem. Abstr. 87 (1977) 58559b].
37. F.M. Shemyakin, O.A. Ofremenko, N.A. Ovesnova, Basic dyes as reagents for drugs of an acidic nature, Farmatsiya (Moscow) 26 (1) (1977) 39-42 [Chem. Abstr. 87 (1977) 58559b].
38. Acar N., Onur F. Spectrophotometric simultaneous analysis of analgin-adamon mixture in injection preparations. Anal. Lett. 29:1996;763-773.
39. Maggiorelli E., Conti L. Identification and determination by spectrophotometry of novalgin with sodium 1,2-naphthoquinone-4-sulfonate. Farmaco (Pavia). 15:1960;179-183.
40. Filipeva S.A., Strelets L.N., Petrenko V.V. Determination of analgin in dosage forms. Farmatsiya (Moscow). 38(1):1989;64-66.
41. Martins M.E.F., Magalhães J.F., Santoro M.I.R.M., Martins J.L.S. Reaction of dipyrone with citral for spectrophotometric determination in pharmaceutical preparations. Rev. Farm. Bioq. Univ. São Paulo. 20(2):1984;133-144.
42. Shingbal D.M., Shirsat P.D. Determination of analgin in pharmaceutical dosage forms. Indian J. Pharm. 37:1975;94-95.
43. Bhatkar R.G., Saldanha M.H. Spectrophotometric determination of analgin. Indian J. Pharm. Sci. 42(5):1980;146-147.
44. A. El-Shanawani, M.F. Metwally, A. El-Bayoumi, M.A. El-Kawi, Determination of dexchlorpheniramine maleate and dipyrone in bulk powder and in pharmaceutical preparations using chloranilic acid as π acceptor, Zhongua Yaoxue Zazhi 44 (5) (1992) 373-379 [Chem. Abstr. 118 (1993) 45901r].
45. A. El-Shanawani, M.F. Metwally, A. El-Bayoumi, M.A. El-Kawi, Determination of dexchlorpheniramine maleate and dipyrone in bulk powder and in pharmaceutical preparations using chloranilic acid as π acceptor, Zhongua Yaoxue Zazhi 44 (5) (1992) 373-379 [Chem. Abstr. 118 (1993) 45901r].
46. Abdine H., Soliman A.S., Morcos M.G. Colorimetric determination of dypirone. J. Pharm. Sci. 62:1973;1834-1836.
47. D.M. Shingbal, A simple method for the estimation of analgin, Indian Drugs Pharm. Ind. 10(5) (1975) 11-12 [Chem. Abst. 85 (1976) 68344a].
48. D.M. Shingbal, A simple method for the estimation of analgin, Indian Drugs Pharm. Ind. 10(5) (1975) 11-12 [Chem. Abst. 85 (1976) 68344a].
49. Pathak V.N., Shukla I.V. Microgram determination of some antipyrines with N-bromosuccinimide. J. Indian Chem. Soc. 60:1983;206-207.
50. K. Kato, M. Umeda, S. Tsubota, Colorimetric determination of sulpyrine in drugs, Yakuzaigaku 24 (1964) 116-119 [Chem. Abstr. 61 (1964) 15936h].
51. K. Kato, M. Umeda, S. Tsubota, Colorimetric determination of sulpyrine in drugs, Yakuzaigaku 24 (1964) 116-119 [Chem. Abstr. 61 (1964) 15936h].
52. Devi M.V., Murthy P.N., Rao M.E.B., Suresh P. Spectrophotometric determination of analgin. East. Pharm. 31:1988;137-138.
53. Kuznetsov V.V., Yakubovich L.M. Determination of sulfonates by color indicating spectrophotometric titration in the analysis of dosage forms. Khim. Farm. Zh. 25(12):1991;62-64.
54. Deffner M., Deffner A.I. Determination of phenylbutazone in pharmaceutical preparations. Chim. Anal. (Paris). 40:1958;460-464.
55. Koupparis M.A., Walczak K.M., Malmstadt H.V. Corticosteroid determination in skin preparations by a reaction rate method. J. Pharm. Sci. 68:1979;1479-1482.
56. Revanasiddappa H.D., Ramappa P.G. Spectrophotometric determinations of some phenothiazine drugs. Talanta. 43:1996;1291-1296.
57. Sastry C.S.P., Srinivas Y., Rao P.V.S. Assay of cisapride in pharmaceutical formulations by extraction spectrophotometry. Talanta. 44:1997;517-526. and Refs. therein.
58. Issa A.S., Beltagy A., Kassen M.G., Daabees H.S. Application of some colorimetric methods for the spectrophotometric determination of phenylbutazone and oxyphenbutazone. Talanta. 32:1985;657-658.
59. Saeed A., Haque H., Qureshi S.Z. Resin bead detection and spectrophotometric determination of oxyphenbutazone with p-dimethylaminocinnamaldehyde - application to bulk drug and dosage forms. Talanta. 40:1993;1867-1871.
60. F. Feigl, Spot Tests in Organic Analysis, fifth ed., Elsevier, Amsterdam, 1956, pp. 331 and 494.
61. Karrer P. Organic Chemistry. fourth ed. 1950;798 Wiley, New York.
62. Georghiou P.E., Ho C.K. The chemistry of the chromotropic acid method for the analysis of formaldehyde. Can. J. Chem. 67:1989;871-876.
63. R. Molinari, A.C. Ikuhara, C.B. Melios, M. Molina, Determinação espectrofotométrica da novalgina (1-fenil, 2,3-dimetil, 4-dimetilaminometano sulfonato de sódio, 5-pirazolona) em medicamentos, Cienc. Cult. (Suppl.) 23(6) (1971) 49 and unpublished results.
64. Mucciarelli S.I.L., Aschieri S.M. Determinación espectrofotométrica de novamin-sulfonato sódico mediante reacción con ácido cromotrópico. Rev. Asoc. Bioq. Arg. 40:1975;79-82.
65. Tubino M., Rossi A.V., Magalhães M.E.A. Quantitative spot tests of Fe(III), Cr(VI) and Ni(II) by reflectance measurements. Anal. Lett. 30:1997;271-282.