Crystal structure of trans- [W(CO)4(n2-C2H4)2] and IR 1H NMR studies of the reactions of this and related ethene carbonyl complexes of tungsten(0), [W(CO)(n)(n2-C2H4)6-(n)] (n = 3-5)

New Journal of Chemistry

Volumn 23, Issue 4, 1999, Pages 407-416

  Szymańska Buzar, Teresa ^a   Kern, Krystyna ^a   Downs, Anthony J ^b   Greene, Timothy M ^b   Morris, Leigh J ^b   Parsons, Simon ^c  

^a UNIVERSITY OF WROC AW   (Poland)

^b UNIVERSITY OF OXFORD   (United Kingdom)

^c UNIVERSITY OF EDINBURGH   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

ARGON; CARBONYL DERIVATIVE; LIGAND; TOLUENE; TUNGSTEN DERIVATIVE;

ARTICLE; CIS TRANS ISOMERISM; COMPLEX FORMATION; CRYSTAL STRUCTURE; INFRARED SPECTROSCOPY; PHOTOCHEMISTRY; PHOTOLYSIS; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; TEMPERATURE DEPENDENCE;

EID: 0032813627     PISSN: 11440546     EISSN: None     Source Type: Journal    
DOI: 10.1039/a808621d     Document Type: Article

References (43)

1. I. W. Stolz, G. R. Dobson and R. K. Sheline, Inorg. Chem., 1963, 2, 1264.
2. M. Wrighton, G. S. Hammond and H. B. Gray, J. Organomet. Chem., 1974, 70, 283.
3. F.-W. Grevels, M. Lindemann, R. Benn, R. Goddard and C. Krüger, Z. Naturforsch., Teil B, 1980, 35, 1298.
4. F.-W. Grevels and V. Skibbe, J. Chem. Soc., Chem. Commun., 1984, 681.
5. K. Angermund, F.-W. Grevels, C. Krüger and V. Skibbe, Angew. Chem., Int. Ed. Engl., 1984, 23, 904.
6. K. R. Pope and M. S. Wrighton, Inorg. Chem., 1985, 24, 2792.
7. M. F. Gregory, S. A. Jackson, M. Poliakoff and J. J. Turner, J. Chem. Soc., Chem. Commun., 1986, 1175.
8. S. A. Jackson, R. K. Upmacis, M. Poliakoff, J. J. Turner, J. K. Burdett and F.-W. Grevels, J. Chem. Soc., Chem. Commun., 1987, 678.
9. F.-W. Grevels, J. Jacke and S. Özkar, J. Am. Chem. Soc., 1987, 109, 7536.
10. B. H. Weiller and E. R. Grant, J. Am. Chem. Soc., 1987, 109, 1252.
11. F.-W. Grevels, J. Jacke, P. Betz, C. Krüger and Y.-H. Tsay, Organometallics, 1989, 8, 293.
12. C. Daniel and A. Veillard, Inorg. Chem., 1989, 28, 1170.
13. S. A. Jackson, P. M. Hodges, M. Poliakoff, J. J. Turner and F.-W. Grevels, J. Am. Chem. Soc., 1990, 112, 1221.
14. P. M. Hodges, S. A. Jackson, J. Jacke, M. Poliakoff, J. J. Turner and F.-W. Grevels, J. Am. Chem. Soc., 1990, 112, 1234.
15. J. A. Banister, S. M. Howdle and M. Poliakoff, J. Chem. Soc., Chem. Commun., 1993, 1814.
16. H. Takeda, M. Jyo-o, Y. Ishikawa and S. Arai, J. Phys. Chem., 1995, 99, 4558.
17. M. Jaroszewski, T. Szymańska-Buzar, M. Wilgocki and J. J. Ziółkowski, J. Organomet. Chem., 1996, 509, 19.
18. T. Szymańska-Buzar, M. Jaroszewski, M. Wilgocki and J. J. Ziółkowski, J. Mol. Catal. A, 1996, 112, 203.
19. T. Szymańska-Buzar, M. Jaroszewski, A. J. Downs, T. M. Greene and L. J. Morris, J. Organomet. Chem., 1997, 531, 207.
20. T. Szymańska-Buzar, K. Kern and D. J. Stufkens, New J. Chem., 1998, 22, 1539.
21. T. Szymańska-Buzar, J. Mol. Catal., 1991, 68, 177.
22. J. M. Dalla Riva Toma, P. H. Toma, P. E. Fanwick, D. E. Bergstrom and S. R. Byrn, J. Crystallogr. Spectrosc. Res., 1993, 23, 41.
23. G. Davidson and C. L. Davies, Inorg. Chim. Acta, 1989, 165, 231.
24. T. Szymańska-Buzar, A. J. Downs, T. M. Greene and A. S. Marshall, J. Organomet. Chem., 1995, 495, 149, 163.
25. (a) G. C. Levy, R. L. Lichter and G. L. Nelson, Carbon-13 Nuclear Magnetic Resonance Spectroscopy, Wiley, New York, 2nd edn., 1980, p. 89;
26. (b) F. A. Bovey, Nuclear Magnetic Resonance Spectroscopy, Academic Press, 2nd edn., 1988, p. 612.
27. G. M. Sheldrick, SHELXL-97, University of Göttingen, 1997.
28. C. Bachmann, J. Demuynck and A. Veillard, J. Am. Chem. Soc., 1978, 100, 2366.
29. E. Hirota, Y. Endo, S. Saito, K. Yoshida, I. Yamaguchi and K. Machida, J. Mol. Spectrosc., 1981, 89, 223.
30. S. Yamamoto, M. Nakata, T. Fukuyama and K. Kuchitsu, J. Phys. Chem., 1985, 89, 3298.
31. D. M. P. Mingos, in Comprehensive Organometallic Chemistry, ed. G. Wilkinson, F. G. A. Stone and E. W. Abel, Pergamon, Oxford, 1982, vol. 3, p. 1; S. D. Ittel and J. A. Ibers, Adv. Organomet. Chem., 1976, 14, 33.
32. D. M. P. Mingos, in Comprehensive Organometallic Chemistry, ed. G. Wilkinson, F. G. A. Stone and E. W. Abel, Pergamon, Oxford, 1982, vol. 3, p. 1; S. D. Ittel and J. A. Ibers, Adv. Organomet. Chem., 1976, 14, 33.
33. (a) R. A. Love, T. F. Koetzle, G. J. B. Williams, L. C. Andrews and R. Bau, Inorg. Chem., 1975, 14, 2653;
34. (b) J. A. K. Howard, J. L. Spencer and S. A. Mason, Proc. R. Soc. London A, 1983, 386, 145;
35. (c) F.-M. Su, C. Cooper, S. J. Geib, A. L. Rheingold and J. M. Mayer, J. Am. Chem. Soc., 1986, 108, 3545;
36. A. J. Schultz, R. K. Brown, J. M. Williams and R. R. Schrock, J. Am. Chem. Soc., 1981, 103, 169.
37. R. N. Perutz and J. J. Turner, J. Am. Chem. Soc., 1975, 97, 4791; Inorg. Chem., 1975, 14, 262; R. N. Perutz, Ph.D. Thesis, University of Cambridge, 1974.
38. R. N. Perutz and J. J. Turner, J. Am. Chem. Soc., 1975, 97, 4791; Inorg. Chem., 1975, 14, 262; R. N. Perutz, Ph.D. Thesis, University of Cambridge, 1974.
39. R. N. Perutz and J. J. Turner, J. Am. Chem. Soc., 1975, 97, 4791; Inorg. Chem., 1975, 14, 262; R. N. Perutz, Ph.D. Thesis, University of Cambridge, 1974.
40. E. Rytter and D. M. Gruen, Spectrochim. Acta, Part A, 1979, 35, 199; D. R. Cowieson, A. J. Barnes and W. J. Orville-Thomas, J. Raman Spectrosc., 1981, 10, 224.
41. E. Rytter and D. M. Gruen, Spectrochim. Acta, Part A, 1979, 35, 199; D. R. Cowieson, A. J. Barnes and W. J. Orville-Thomas, J. Raman Spectrosc., 1981, 10, 224.
42. B. McNamara, D. M. Becher, M. H. Towns and E. R. Grant, J. Phys. Chem., 1994, 98, 4622.
43. J. C. Linehan, C. R. Yonker, J. T. Boys, S. T. Autrey, T. E. Bitterwolf and S. Gallagher, J. Am. Chem. Soc., 1998, 120, 5826.