Synthesis and NMR investigation of 3,4-diazabicyclo[4.3.0]non-2-ene and N,N'-azo-3-azabicyclo[3.3.0]octane. X-ray crystal structure analysis of a new tetrazene derivative

Journal of Heterocyclic Chemistry

Volumn 36, Issue 3, 1999, Pages 681-686

  Delalu, H ^a   Elkhatib, M ^a   Peyrot, L ^a   Fenet, B ^a   Mentzen, B F ^b  

^a UNIVERSITÉ LYON 1   (France)

^b UNIVERSITÉ CLAUDE BERNARD LYON 1   (France)

Author keywords

[No Author keywords available]

Indexed keywords

3,4 DIAZABICYCLO[4.3.0]NON 2 ENE; ALICYCLIC COMPOUND; BICYCLO[3.3.0]OCTANE DERIVATIVE; N,N' AZO 3 AZABICYCLO[3.3.0]OCTANE; TETRAZENE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CIS TRANS ISOMERISM; CRYSTAL STRUCTURE; DRUG SYNTHESIS; NUCLEAR MAGNETIC RESONANCE; OXIDATION; X RAY CRYSTALLOGRAPHY;

EID: 0032810964     PISSN: 0022152X     EISSN: None     Source Type: Journal    
DOI: 10.1002/jhet.5570360317     Document Type: Article

References (10)

1. S. Ehrreich and L. Zitowitz, German offen. 2,415,064 (1974); Chem. Abstr., 82, 4115g (1975).
2. M. Elkhatib, Thèse de Doctorat no89-94, Lyon, 1994, 186 pp.
3. A. W. Rytina, R. W. Schiessler and F. C. Whitmore, J. Am. Chem. Soc., 71, 751 (1949).
4. D. M. Dodrell, D. T. Pegg and M. R. Bendall, J. Magn. Reson., 48, 323 (1982).
5. R. Cohen-Adad, H. Delalu and H. Sautereau, French Demande 2,383,916 (1977); Chem. Abstr., 91, 19887V (1979).
6. R. Cohen-Adad, A. Cohen, H. Delalu, A. Marchand and A. Maugé, S. African ZA 87 04,526 (1987); Chem. Abstr., 109, 131251z (1988).
7. H. Delalu and A. Marchand, Anal. Chim. Acta, 266, 39 (1992).
8. G. M. Sheldrick, SHELXS-86, a program for the solution of crystal structures from diffraction data, Acta Crystallogr., A46, 467 (1990).
9. G. M. Sheldrick, SHELXL-93, a program for the refinement of crystal structures from diffraction data.
10. M. N. Burnett and C. K. Johnson, ORTEP-III, Oak Ridge thermal ellipsoid plot program for crystal structure illustrations, ORNL-6895 report, PC and Apple Macintosh 1996 versions.