Molecular, crystal and solution structure of a β-cyclodextrin complex with the bromide salt of 2-(3-dimethylaminopropyl)tricyclo[3.3.1.13,7]decan-2-ol, a potent antimicrobial drug

Carbohydrate Research

Volumn 317, Issue 1-4, 1999, Pages 19-28

  Perrakis, Anastassis ^a   Antoniadou Vyza, Ekaterini ^b   Tsitsa, Polyxeni ^b   Lamzin, Victor S ^c   Wilson, Keith S ^c   Hamodrakas, Stavros J ^b  

^a EUROPEAN MOLECULAR BIOLOGY LABORATORY   (France)

^b Univ A   (Greece)

^c EUROPEAN MOLECULAR BIOLOGY LABORATORY   (Germany)

Author keywords

Cyclodextrin; Ab initio structure solution; Antimicrobial drug; NMR; Synchrotron radiation; X ray crystallography

Indexed keywords

ADAMANTANE DERIVATIVE; ANTIINFECTIVE AGENT; BETA CYCLODEXTRIN DERIVATIVE;

ARTICLE; CHEMICAL STRUCTURE; COMPLEX FORMATION; CONFORMATION; CRYSTAL STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRIORITY JOURNAL; TEMPERATURE; X RAY CRYSTALLOGRAPHY;

ANTI-BACTERIAL AGENTS; BACTERIA; BETA-CYCLODEXTRINS; BROMIDES; CARBOHYDRATE CONFORMATION; CRYSTALLOGRAPHY, X-RAY; CYCLODEXTRINS; FATTY ALCOHOLS; MODELS, MOLECULAR; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR;

EID: 0032796996     PISSN: 00086215     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0008-6215(99)00021-X     Document Type: Article

References (24)

1. J. Szeijtli, Cyclodextrin Technology, Kluwer, Academic Publishers (1989).
2. Saenger W. Angew. Chem., Int. Ed. Engl. 19:1980;344-362.
3. Saenger W. Isr. J. Chem. 25:1985;43-50.
4. Tsitsa P., Berghe D.A. Eur. J. Med. Chem. 28:1993;149-158.
5. S.C. Harvey, in A.G. Gilman, L.S. Goodman, A. Gilman (Eds.), Goodman and Gilman's The Pharmacological Basis of Therapeutics, 6th ed., Macmillan, New York, 1980, pp. 978-979.
6. D. Cremer, J.A. Pople, J. Am. Chem. Soc., 97 (1975) 1354-1358.
7. Z. Hajek, Vodicka, Z. Ksandr, S. Landa, Tetrahedron Lett., 40 (1972) 4103-4106.
8. van Deursen F.W., Korver P.K. Tetrahedron Lett. 40:1967;3923-3928.
9. van Deursen F.W., Bakker J. Tetrahedron. 27:1971;4593-4600.
10. Lamzin V.L., Wilson K.S. Acta Crystallogr. D50:1993;129-147.
11. A. Perrakis, T.K. Sixma, K.S. Wilson, V.S. Lamzin (1997) in Recent advances in phasing, Proceedings of Daresbury study weekend.
12. CCP4 Acta Crystallogr., D50 (1994) 760-763.
13. Grochowski J., Serda P., Wilson K.S., Dauter Z. J. Appl. Cryst. 22:1994;722-726.
14. Perrakis A., Schneider T., Antoniadou-Vyzas E., Dauter Z., Hamodrakas S.J. J.Appl.Cryst. 29:1996;261-264.
15. A. Arndt, A.J. Wonacott, The Rotation Method in Crystallography, North Holland Publishing Company, Amsterdam, 1977, pp. 75-103.
16. Z. Otwinowski, DENZO: An oscillation data processing program for macromolecular crystallography, Yale University, New Haven, USA, 1993.
17. Kottke D., Stalke D. J. Appl. Cryst. 26:1993;615-619.
18. J. Cosier, A.M. Glazer, J. Appl. Cryst., (1986) 105-107.
19. G.M Sheldrick, Shelxs-86, Program for the solution of Crystal Structures. Univ. of Gottingen, Germany, 1985.
20. G. Murshudov, A. Vagin, E. Dodson, (1996) Application of maximum likelihood refinement, in The refinement of protein structures, Proceedings of Daresbury study weekend.
21. G.M Sheldrick, Shelxl-93, Program for Crystal Structure refinement. Univ. of Gottingen, Germany, 1993.
22. Jones A. Acta Crystallogr. A47:1991;110-119.
23. A.L. Spek, PLATON-92, Univ. of Utrecht, The Netherlands, 1992.
24. Kraulis P.J. J. Appl. Cryst. 24:1996;946-950.