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0345378161
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note
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1H NMR spectrum of the crude concentrated product after the usual workup in each case indicated the presence of at least 60% of the unreacted keto ester, formation of the desired product 6 in low yield (<10%), formation of the dimer of mvk i.e. 3-methylene-2,6-heptanedione as a major product, and some other side products).
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0032564002
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Watanabe, S.5
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23
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0344515988
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note
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4; C, 67.73; H, 6.50; found: C, 67.55; H, 6.51.
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