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85034138922
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note
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Spontaneous oligomerization of 1 is still observed in the presence of the chlorotrimethylsilane, but the oligomers appear to be silylated as confirmed by elemental analysis.
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17
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85034146873
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note
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Significant losses of 1 occurred when chlorotrimethylsilane was distilled off and through oligomerization during transfers.
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18
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84916160705
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The thermal polymerization of phenylacetylene is well known to be a radical process; Chauser, M. G.; Rodionov, Y. M.; Misin, V. M.; Cherkashin, M. I. Russ Chem Rev 1976, 45, 348.
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20
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84989427699
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0020846489
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25
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85034145758
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note
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C = 325 ppm (see ref. 22).
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26
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0001597278
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Nguyen, T.; Landuyt, L.; Vanquickenborne, L. G. J Org Chem 1993, 58, 2817.
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