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The crystallographic data (without structural factors) of the structures described in this publication were deposited as "supplementary publications no. CCDC 101981 (21), 102125 (33), and 102146 (rac-48)" at the Cambridge Crystallography Data Centre. Copies of the data can be obtained with no charge from the following address in Great Britain: The Director, CCDC, 12 Union Road, Cambridge CB2 1EZ (Telefax Int. + 1223/336-033; E-mail: deposit@ccdc.cam.ac.uk).
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0344756687
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As only a small amount of 44 had been prepared for the NOE measurement, the compound was not completely characterized.
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The identity of 8 has qualitatively been confirmed by an X-ray crystal structure analysis. However, the quality of the crystals was not sufficient to obtain an analysis of publishable quality.
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