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23
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0344295659
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note
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1H NMR spectra of the products remained consistent with the composition calculated for 7a and Tb.
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24
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0344727728
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note
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31P NMR spectrum ourselves in THF. The material was kindly provided by Digital Specialty Chemicals, Ltd.
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26
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0000307158
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Graff, J. L.; Sanner, R. D.; Wrighton, M. S. Organometallics 1982, 1, 837.
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27
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0000040311
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The synthesis of [1]phosphaferrocenophane 1 has been previously described. See: (a) Osborne, A. G.; Whiteley, R. H.; Meads, R. E. J. Organomet. Chem. 1980, 793, 345.
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33846550091
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30
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0345590048
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note
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1H NMR integration assuming full conversion of 1 to living polymer 4.
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