Synthesis and crystal structure of an O-silylated hexahomotriazacalix[3]arene

Tetrahedron Letters

Volumn 39, Issue 31, 1998, Pages 5473-5476

  Chirakul, Panadda ^a   Hampton, Philip D ^a   Duesler, Eileen N ^a  

^a UNIVERSITY OF NEW MEXICO   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

1 TRIMETHYLSILYLIMIDAZOLE; 1,1,1,3,3,3 HEXAMETHYLDISILAZANE; BIS(TRIMETHYLSILYL)TRIFLUOROACETAMIDE; HEXAHOMOTRIAZACALIX[3]ARENE; UNCLASSIFIED DRUG;

ARTICLE; CRYSTAL STRUCTURE; HYDROGEN BOND; METHODOLOGY; STRUCTURE ANALYSIS; SYNTHESIS;

ARENE;

EID: 0032581729     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(98)01136-8     Document Type: Article

References (11)

1. 1. Hampton, P. D.; Tong, W.; Wu, S.; Duesler, E. N. J Chem. Soc., Perkin Trans. 2. 1996, 1127-1130.
2. 2. a) Gutsche, C. D.; Levine, J. A. J. Amer. Chem. Soc. 1982, 104, 2652-2653;
3. b) Gutsche, C. D.; Dhawan, B.; Levine, J. A.; Hyun, N. K.; Bauer, L. J. Tetrahedron 1983, 39, 409-426;
4. c) Gutsche, C. D.; Bauer L. J. J. Amer. Chem. Soc. 1985, 107, 6059-6063;
5. d) Gutsche, C. D.; Pagoria, P. F. J. Org. Chem. 1985, 50, 5795-5802.
6. 3. Ikeda, A.; Shinkai, S. Chem. Rev. 1997, 97, 1713-1734.
7. 4. Takemura, H.; Shinmyozu, T.; Miura, H.; Khan, I. U.; Inazu, T. J. Incl. Phenom. Mol. Recogn. 1994, 19, 193-206.
8. 5. Takemura, H; Shinmyozu, T.; Inazu, T. J. Coordination Chem. 1996, 156, 183-200.
9. 6. Hampton, P. D.; Daitch, C. E.; Duesler, E. N. New J. Chem. 1996, 20, 427-437.
10. w were 6.80, 5.88% for the observed data.
11. 3, 125 MHz) δ 172.5, 148.5, 130.4, 130.2, 129.6, 129.4, 129.2, 58.5, 52.5, 20.6, 20.0, 1.1.