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For more recent examples see: d) Kurihara, M.; Ito, S.; Tsutsumi, N.; Miyata, N. Tetrahedron Lett., 1994, 35, 1577.
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4. a) Mello, R.; Fiorentino, M.; Sciacovelli, O.; Curci, R. J.Org.Chem., 1988, 53, 3890.
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c) Mello, R.; Cassidei, L.; Fiorentino, M.; Fusco, C.; Curci, R. Tetrahedron Lett., 1990, 31, 3067.
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d) Altamura, A.; Fusco, C.; D'Accolti, L.; Mello, R.; Prencipe, T.; Curci, R. Tetrahedron Lett., 1991, 32, 5445.
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5. Brown, D.S.; Marples, B.A.; Smith, P.; Walton, L. Tetrahedron, 1995, 51, 3587.
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7. Trifluoroacetophenone has been reported as a catalyst in the oxidation of sulphides in the presence of bovine serum albumin (Colonna.S.; Gaggero, N.; Leone, M. Tetrahedron Lett., 1991, 47, 8385.)
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18
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36949027247
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8. 4-(Trifluoroacetyl) benzoic acid was supplied by Lancaster and was also synthesised by the published procedure (Chen, L.S.; Chen, G.J.; Tamborski, C. Journal of Organometallic Chemistry, 1983, 251, 139).
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0010628481
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note
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10. The hydroxymethyl resin [01-64-0110] was obtained from Novabiochem with a reported loading of 1.16mMols/g; isolation of the acid from the resin showed that the resin was in fact 33% substituted. The TentaGel S-Br resin [O-(2-Bromoethyl)polyethylene glycol polymer bound] is available from Fluka with a reported loading of ≈ 0.26 mmol Br/g; isolation of the acid from the resin showed that the resin was in fact 50% substituted.
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