New one-pot synthesis of tetra- alkoxycarbonylallylidenetriphenylphosphoranes

Tetrahedron Letters

Volumn 39, Issue 9, 1998, Pages 1051-1054

  Yavari, Issa ^a   Baharfar, Robabeh ^a  

^a TARBIAT MODARES UNIVERSITY   (Iran)

Author keywords

[No Author keywords available]

Indexed keywords

CARBOXYLIC ACID DERIVATIVE; LACTONE; PHOSPHORANE DERIVATIVE; TETRA ALKOXYCARBONYLALLYLIDENETRIPHENYLPHOSPHORANE; UNCLASSIFIED DRUG;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; COMPLEX FORMATION; DRUG ELIMINATION; DRUG SYNTHESIS; NONHUMAN; OXIDATION; PROTON TRANSPORT; REACTION ANALYSIS;

EID: 0032568045     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)10725-0     Document Type: Article

References (10)

1. 1. Yavari, I. and Baharfar, R. Tetrahedron Lett., 1997, 38, 4259-4262.
2. 2. Hudson, H. R., in "The Chemistry of Organophosphorus Compounds, Volum I. Primary, Secondary and Tertiary Phosphines, Polyphosphines and Heterocyclic Organophosphorus (III) Compounds," (Ed.: Hartley, F. R.), Wiley, New York, 1990, pp. 386-472.
3. 3. Bestmann, H. J. and Zimmermann, R., Topics Curr. Chem. 1971, 20, 1-141.
4. 4. Dimorth, K., Topics Curr. Chem. 1973, 38, 1-147.
5. 5. Corbridge, D. E. C. "Phosphorus, An Outline of the Chemistry, Biochemistry and Uses", 5th ed., Elsevier, 1995, Amsterdam.
6. 6. Wasserman, H. H. Baldino, C. M. and Coats, S. J. J. Org. Chem., 1995, 60, 8231.
7. 7. Manouni, D. El. Leroux, Y. and Burgada, R. Tetrahedron Lett., 1986, 42, 2435.
8. 8P requires C, 67.11; H, 5.97%).
9. 9. We have used triethylamine to mop-up the HX. However, this complicates the work-up process and increases the yield hardly at all.
10. 10. Gunther, H. NMR Spectroscopy, 2nd ed., Chapt. 9. Wiley, New York, 1995.