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Volumn 63, Issue 26, 1998, Pages 9910-9918

Total synthesis of (±)-quinolizidine 217A

Author keywords

[No Author keywords available]

Indexed keywords

1 METHYL 4 (PENT 2 EN 4 YNYL)QUINOLIZIDINE; QUINOLIZIDINE 217A; QUINOLIZIDINE DERIVATIVE; UNCLASSIFIED DRUG;

EID: 0032567397     PISSN: 00223263     EISSN: None     Source Type: Journal    
DOI: 10.1021/jo981695d     Document Type: Article
Times cited : (43)

References (37)
  • 2
    • 0011838270 scopus 로고
    • Cordeil, G. A., Ed.; Academic Press: San Diego
    • (b) Daly, J. W.; Garraffo, H. M.; Spande, T. F. In The Alkaloids; Cordeil, G. A., Ed.; Academic Press: San Diego, 1993; Vol. 43, pp 185-288.
    • (1993) The Alkaloids , vol.43 , pp. 185-288
    • Daly, J.W.1    Garraffo, H.M.2    Spande, T.F.3
  • 3
    • 0004237729 scopus 로고    scopus 로고
    • Cordell, G. A., Ed.; Academic Press: New York
    • Daly, J. In The Alkaloids; Cordell, G. A., Ed.; Academic Press: New York, 1997; Vol. 50.
    • (1997) The Alkaloids , vol.50
    • Daly, J.1
  • 30
    • 33847526300 scopus 로고    scopus 로고
    • Personal communication with John \V. Daly and T. Spande, NIDDK (National Institutes of Health). The GC-FTIR data was obtained on an HP-5 fused silica-bonded capillary column (25 m × 0.32 mm). The chiral GC analysis was performed using a Supelco Beta-DEX 120 fused silica capillary column (30 m, 0.25 mm i.d., 0.25 μm film thickness)
    • Personal communication with John \V. Daly and T. Spande, NIDDK (National Institutes of Health). The GC-FTIR data was obtained on an HP-5 fused silica-bonded capillary column (25 m × 0.32 mm). The chiral GC analysis was performed using a Supelco Beta-DEX 120 fused silica capillary column (30 m, 0.25 mm i.d., 0.25 μm film thickness).
  • 36
    • 20644467542 scopus 로고    scopus 로고
    • note
    • In a separate experiment, chromatography of the imine 28 was attempted (2:1 ethyl acetate/hexane followed by methanol/chlorofonn). Although a pure sample of 28 could not be obtained due to its decomposition, an impure byproduct was isolated in 15% yield that had spectral data consistent with an aziridine. This material exhibited the same multiplet at δ 5.2 ppm as that observed in the sealed tube experiments.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.