Preparation of ω-tetrahydropyran-2-ylsulfanylalkylmagnesium chlorides: Useful reagents for the synthesis of 1-(ω-mercaptoalkyl)-1,2- dihydrobuckminsterfullerenes (C60)

Tetrahedron Letters

Volumn 39, Issue 52, 1998, Pages 9693-9696

  Kim, Sung Hoon ^a   Lee, Sung Han ^a   Kang, Seung Hoon ^a  

^a Konkuk University   (South Korea)

Author keywords

[No Author keywords available]

Indexed keywords

FULLERENE DERIVATIVE; TETRAHYDROPYRAN DERIVATIVE;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; MOLECULAR STABILITY; PROTON NUCLEAR MAGNETIC RESONANCE; REACTION ANALYSIS; SYNTHESIS;

EID: 0032564607     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(98)02142-X     Document Type: Article

References (19)

1. 1. General reference for Grignard reagents; "Organomagnesium Methods in Organic Synthesis" B. J. Wakefield, Academic Press, 1995
2. 2. A. Greiner Tetrahedron Lett., 1989, 30, 3547
3. 3. A. Maercker and H. Jaroschek J. Organometallic Chem. 1976, 116, 21
4. 4. H. Sakurai, M. Kira and M. Kumeda Chem. Commun. 1967, 889
5. 5. H. Normant, and B. Castro C. R. Acad Sc. Paris 1964, 259, 830
6. 6. W. Krätschmer, K. Fostiropoulos, R. Huffman Nature 1990, 347, 354
7. 7. K. Chen, W. B. Caldwell, C. A. Mirkin J. Am. Chem. Soc. 1993, 115, 1193
8. 8. G. Schick, K. Kampe, A. Hirsch J. Chem. Soc., Chem. Commun. 1995, 2023
9. 9. M. Keshavarz-K, B. Knight, G. Srdanov, F. Wudl J. Am. Chem. Soc. 1995, 117, 11371
10. 10. K. Mikami, S. Matsumoto, A. Ishida, S. Takamuku T. Suenobu, S. Fukuzumi J. Am. Chem. Soc. 1995, 117, 11134
11. 11. J. R. Morton, K. F. preston, P. J. Krusic, S. A. Hill, E. Wasserman J. Am. Chem. Soc. 1992, 114, 5454
12. 12. P. J. Krusic, E. Wasserman, P. N. Keizer, J. R. Morton, K. F. Preston Science 1991, 254, 1183
13. 13. A. Hirsch, T. Grosser, A. Soi Chem. Ber. 1993, 126, 1061
14. 14. H. Nagashima, H. Terrasaki, E. Kimura, K. Nakajima, K. Itoh J. Org. Chem. 1994, 59, 1246
15. 15. P. J. Fagan, P. J. Krusic, D. H. Evans, S. A. Lerke, E. Johnston J. Am. Chem.Soc. 1992, 114, 9697
16. 16. G. Wang, Y. Murata, K. Komatsu, T. S. M. Wan Chem. Commun. 1996, 2059
17. 17. X. Shi, W. B. Caldwell, K. Chen, C. A. Mirkin J. Am. Chem. Soc. 1994, 116, 1598
18. 18. T. Ehler, N. Malmberg, L. J. Noe J. Phys. Chem. B. 1997, 101, 1268 and references there in.
19. max = 211, 257, 323, 431, 659 nm