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2 (5:1), resulting in colorless crystals of 2 (7.6 g, 58 %); mp 128 °C.
-
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18
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0031591341
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84943920736
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-3 (1.04 Å from F6). Atomic coordinates and e.s.d.'s for both crystal structures (6 and 7) have been deposited at the Cambridge Crystallographic Data Centre.
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SHELXL-97
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Sheldrick, G.M.1
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23
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0010257052
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note
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2 prior to analysis by gas chromatography.
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24
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84956118821
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