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0010295647
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note
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(6) The details of the preparation of the starting enynes 3 will appear eleswhere accompanied with the experiments on its Pauson-Khand reaction in due course.
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15
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0000795340
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Schreiber, S.L.3
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18
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0010242954
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note
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1H NMR spectrum of 4c(β) showed a smaller coupling constant (3.4 Hz) between the H-2 and H-3 due to an equatorial-equatorial coupling, while an axial-axial coupling constant (8.3 Hz) was recorded for 4c(α). Furthermore an NOE experiment with 4c(α) revealed a 3.8% enhancement between H-2 and H-6. No enhancement could be observed between these two protons in 4c(β).
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19
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0010296984
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note
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(11) (1S,2S,3E)-3-Benzylidene-1,2-bis(tert-butyldimethylsilyloxy)-4-methylenecyclohexane was obtained in 27% yield as a by-product.
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21
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33745353321
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(b) Magnus, P.; Exon, C.; Albaugh-Robertson, P. Tetrahedron, 1985, 41, 5861.
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Magnus, P.1
Exon, C.2
Albaugh-Robertson, P.3
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22
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0010267845
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note
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2.
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