Nuclei breeding from a chiral crystal seed of NaClO3

Chemical Engineering Science

Volumn 53, Issue 9, 1998, Pages 1745-1756

  Qian, Ru Ying ^a   Botsaris, Gregory D ^a  

^a Tufts University   (United States)

Author keywords

Nucleation dispersion; Nucleation mechanism; Nuclei chirality; Secondary nucleation; Sodium chlorate

Indexed keywords

COAGULATION; COOLING; CRYSTALLIZATION; SODIUM COMPOUNDS;

EMBRYOS COAGULATION SECONDARY NUCLEATION (ECSN); NUCLEI BREEDING; NUCLEI CHIRALITY; SODIUM CHLORATE;

NUCLEATION;

EID: 0032557522     PISSN: 00092509     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0009-2509(98)00040-2     Document Type: Article

References (14)

1. Davey R. J., Black S. N., William L. J., McEwan D., Sadler D. E. The chiral purity of a triazolylketone crystallized from racemic solution. J. Crystal Growth. 102:1990;97-102.
2. Denk E. G., Botsaris G. D. Fundamental studies in secondary nucleation. J Crystal Growth. 13/14:1972;493-499.
3. Kondepudi D. K., Bullock K. L., Digits J. A., Hall J. K., Miller J. M. Kinetics of chiral symmetry breaking in crystallization. J. Am. Chem. Soc. 115:1993;10,211-10,216.
4. Kondepudi D. K., Bullock K. L., Digits J. A., Yarborough P. D. Stirring rate as a critical parameter in chiral symmetry breaking crystallization. J. Am. Chem. Soc. 117:1995;401-404.
5. Kondepudi D. K., Kaufman R. J., Singh N. Chiral symmetry breaking in sodium chlorate crystallization. Science. 250(4983):1990;975-977.
6. Kuznestov Yu.G., Malkin A. J., Glantz W., McPherson A. In situ atomic force microscopy studies of protein and virus crystal growth mechanisms. J. Crystal Growth. 168:1996;63-73.
7. McBride J. M., Carte R. L. Spontaneous formation of enantiomorphic crystals with stirring. Angew. Chem. Int. Ed. Engl. 30:1991;293-295.
8. Qian R. Y., Botsaris G. D. A new mechanism for nuclei formation in suspension crystallizers. the role of interparticle forces Chem. Engng Sci. 52:1997;3429-3440.
9. Randolph, A. D. and Larson, M. A. (1988) Theory of Particulate Processes: Analysis and Techniques of Continous Crystallization, 2nd edn. Academic Press, San Diego, pp. 126-129.
10. Ristic R. I., Sherwood J. N., Wojciechowski K. Assessment of the strain in small sodium chlorate crystals and its relation to growth rate dispersion. J. Crystal Growth. 91(1/2):1988;163-168.
11. Ristic R. I., Sherwood J. N., Wojciechowski K. The assessment of strain in material using synchrotron radiation techniques and the role of strain in growth rate dispersion. J. Crystal Growth. 144(1/2):1994;87-90.
12. Saratovkin, D. D. (1959) Dendritic Crystallization. pp. 64-65. Consultants Bureau, New York.
13. Yokota M., Oguchi T., Arai K., Toyokura K., Inoue C., Naijyo H. Growth rate of S-carboxymethyl-D-cysteine and its optical resolution. Myerson A. S., Toyokura K. Crystallization as a Separations Process. 1990;271-280 ACS, Washington D.C., USA. ACS Symposium No. 438.
14. Yokota, M. and Toyokura, K. (1992) Heterogeneous nucleation of D-SCMC on the surface of L-SCMC crystal. Paper presented at the AIChE 1992 Annual Meeting, Paper No. 20h, November 1-6, Miami Beach, Florida.