First synthesis and structural characterisation of a tertiary phosphine containing an azo linkage

Tetrahedron Letters

Volumn 39, Issue 21, 1998, Pages 3571-3574

  Alder, Mark J ^a   Flower, Kevin R ^a   Pritchard, Robin G ^a  

^a UNIVERSITY OF MANCHESTER   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

AZO COMPOUND; OXIDE; PHOSPHINE DERIVATIVE;

ARTICLE; CHEMICAL STRUCTURE; PROTON NUCLEAR MAGNETIC RESONANCE; SYNTHESIS; X RAY DIFFRACTION;

EID: 0032554956     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(98)00551-6     Document Type: Article

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14. 2 = 0.106 (all data), T = 123 K, Enraf- Nonius FAST diffractometer, λ = 0.71069 Å. Full least- squares refinement with SHELXL-97, H atoms in riding mode and all non-hydrogen atoms anisotropic. Atomic coordinates, bond lengths and angles and thermal parameters have been deposited at the Cambridge Crystallographic Data Centre (CCDC).
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