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0344950037
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note
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3I, was excluded by NMR spectroscopy and mass spectrometry. In our opinion the enlarged motion parameter can be explained solely by the low coordination number of the thallium atom. Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Center as supplementary publication no. CCDC-100750. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: (+44)1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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