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0345381501
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note
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2O (Yield: 6.7 g, 82%). EIMS: m/z = 392. Satisfactory analytical and NMR spectral data were obtained.
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29
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0345381498
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note
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4 resulted in-precipitation of the complexes, which were filtered off, washed with MeOH. and dried in vacuo to give the complexes in 80-90% yield. Satisfactory analytical data (C, H, N) were obtained for both.
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0344950006
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note
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-3. This crystal diffracted very weakly. To assist in the refinement, several restraints were applied: 1) all aromatic rings were restrained to be flat; 2) in the tetrafluoroborate anions all B-F bonded and all F⋯F nonbonded distances were restrained to be similar: 3) thermal parameters on adjacent atoms were restrained to be similar. c) Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-100861. Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: (+44) 1223-336-033; e-mail: deposit@chemcrys.cam.ac.uk).
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Reuter, H.2
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A. Müller, H. Reuter, S. Dillinger, Angew. Chem. 1995, 107, 2505; Angew. Chem. Int. Ed. Engl. 1995, 34, 2328.
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Z. Hou, C. J. Sunderland, T. Nishio, K. N. Raymond, J. Am. Chem. Soc. 1996, 118, 5148.
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Raymond, K.N.4
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35
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0345381499
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note
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- anions and the paramagnetism of the cavity.
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