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33646082281
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note
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2 with all data (SHELXL95), 1102 parameters. H atoms were placed in calculated positions with the conformational orientation of MeCN methyl hydrogen atoms deduced from circular Fourier syntheses, GOF = 0.964, R = 0.065, wR (all data) = 0.198. Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-101 615. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK deposit@ccdc.cam.ac.uk
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