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Volumn 39, Issue 16, 1998, Pages 2231-2234

Expanded cyclophanes Part 1. Synthesis and structure of 4,17- dithia[7.7]metacyclophane-1,6,14,19-tetrayne

Author keywords

[No Author keywords available]

Indexed keywords

4,17 DITHIA[7.7]METACYCLOPHANE 1,6,14,19 TETRAYNE; BROMOBENZOIC ACID DERIVATIVE; UNCLASSIFIED DRUG;

EID: 0032537089     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(98)00233-0     Document Type: Article
Times cited : (6)

References (21)
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    • 1. Bodwell, G. J., Bridson, J. N., Houghton, T. J., Kennedy, J. W. J., Mannion, M. R. Angew. Chem. 1996, 108, 1418-1420; Angew. Chem. Int. Ed. Engl. 1996, 35, 1320-1321.
    • (1996) Angew. Chem. Int. Ed. Engl. , vol.35 , pp. 1320-1321
  • 4
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    • 2. Bodwell, G. J., Houghton, T. J., Kennedy, J. W. J., Mannion, M. R. Angew. Chem. 1996, 108, 2280-2281; Angew. Chem. Int. Ed. Engl. 1996, 35, 2121-2123.
    • (1996) Angew. Chem. Int. Ed. Engl. , vol.35 , pp. 2121-2123
  • 5
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    • Academic Press, New York
    • 3. a) Keehn, P. M., Rosenfeld, S. M. (Eds.), Cychphanes, Vols. 1 and 2, Academic Press, New York, 1983;
    • (1983) Cychphanes , vol.1-2
    • Keehn, P.M.1    Rosenfeld, S.M.2
  • 7
    • 0003825877 scopus 로고
    • Royal Society of Chemistry, London
    • c) F. N. Diederich, Cyclophanes, Royal Society of Chemistry, London, 1991.
    • (1991) Cyclophanes
    • Diederich, F.N.1
  • 9
    • 33750436741 scopus 로고
    • 4. Hopf, H., Jones, P. G, Bubenitschek, P., Werner, C. Angew. Chem. 1995, 107, 2592-2594; Angew. Chem. Int. Ed. Engl. 1995, 34, 2367-2368.
    • (1995) Angew. Chem. Int. Ed. Engl. , vol.34 , pp. 2367-2368
  • 11
    • 0010732904 scopus 로고    scopus 로고
    • note
    • f = 0.26, 40 mg, 11%).
  • 12
    • 0010732419 scopus 로고    scopus 로고
    • note
    • 5 IR (nujol) C=C not observed; Calcd. C 78.22, H 4.38; Found C 77.95, H 4.38.
  • 14
    • 0010732748 scopus 로고    scopus 로고
    • note
    • w = 0.035, GOF 1.73.
  • 15
    • 0010647590 scopus 로고
    • 10. A search of the Cambridge Crystallographic Database afforded only two reported crystal structures of anti-2,11-dithia[3.3]metacyclophanes: a) Chan, T.-L., Chan, C.-K., Ho, K.-W., Tse, J. S., Mak, T. C. W. J. Cryst. Mol. Struct. 1977, 7, 199-205;
    • (1977) J. Cryst. Mol. Struct. , vol.7 , pp. 199-205
    • Chan, T.-L.1    Chan, C.-K.2    Ho, K.-W.3    Tse, J.S.4    Mak, T.C.W.5
  • 18
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    • 12. Sako, K., Hirakawa, T., Fujimoto, N., Shinmyozu, T., Inazu, T., Horimoto, H. Tetrahedron Lett. 1988, 29, 6275-6278; Sako, K., Takemura, H., Suenaga, M., Shinmyozu, T., Inazu, T., J. Org. Chem. 1992, 57, 6536-6541; Semmelhack, M. F., Harrison, J. J., Young, D. C., Gutiérrez, A., Rafii, A. S., Clardy, J. J. Am. Chem. Soc. 1989, 707, 7508-7514.
    • (1988) Tetrahedron Lett. , vol.29 , pp. 6275-6278
    • Sako, K.1    Hirakawa, T.2    Fujimoto, N.3    Shinmyozu, T.4    Inazu, T.5    Horimoto, H.6
  • 19
    • 0000426203 scopus 로고
    • 12. Sako, K., Hirakawa, T., Fujimoto, N., Shinmyozu, T., Inazu, T., Horimoto, H. Tetrahedron Lett. 1988, 29, 6275-6278; Sako, K., Takemura, H., Suenaga, M., Shinmyozu, T., Inazu, T., J. Org. Chem. 1992, 57, 6536-6541; Semmelhack, M. F., Harrison, J. J., Young, D. C., Gutiérrez, A., Rafii, A. S., Clardy, J. J. Am. Chem. Soc. 1989, 707, 7508-7514.
    • (1992) J. Org. Chem. , vol.57 , pp. 6536-6541
    • Sako, K.1    Takemura, H.2    Suenaga, M.3    Shinmyozu, T.4    Inazu, T.5
  • 20
    • 0001724196 scopus 로고
    • 12. Sako, K., Hirakawa, T., Fujimoto, N., Shinmyozu, T., Inazu, T., Horimoto, H. Tetrahedron Lett. 1988, 29, 6275-6278; Sako, K., Takemura, H., Suenaga, M., Shinmyozu, T., Inazu, T., J. Org. Chem. 1992, 57, 6536-6541; Semmelhack, M. F., Harrison, J. J., Young, D. C., Gutiérrez, A., Rafii, A. S., Clardy, J. J. Am. Chem. Soc. 1989, 707, 7508-7514.
    • (1989) J. Am. Chem. Soc. , vol.707 , pp. 7508-7514
    • Semmelhack, M.F.1    Harrison, J.J.2    Young, D.C.3    Gutiérrez, A.4    Rafii, A.S.5    Clardy, J.6
  • 21
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    • in reference 3a, Vol. 1, Ch. 4, p. 239-310, and references cited therein
    • 13. Mitchell, R. H. in reference 3a, Vol. 1, Ch. 4, p. 239-310, and references cited therein.
    • Mitchell, R.H.1


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