1,8-Diazabicyclo[6.6.4]octadeca-4,11,16-triyne. A bridgehead amine with planar nitrogens

Tetrahedron Letters

Volumn 39, Issue 7, 1998, Pages 513-516

  Wolfart, Volker ^a   Gleiter, Rolf ^a   Krieger, Claus ^b   Pritzkow, Hans ^a  

^a UNIVERSITY OF HEIDELBERG   (Germany)

^b Abt Chem des Max Planck I   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

AMINE; BICYCLO COMPOUND; NITROGEN;

ARTICLE; CONFORMATION; CRYSTAL STRUCTURE; SYNTHESIS; X RAY ANALYSIS;

EID: 0032510083     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)10626-8     Document Type: Article

References (13)

1. 1 Alder, R.W. Acc. Chem. Res. 1983, 16, 321; Tetrahedron 1990, 46, 683; Alder, R.W. ; East, S. P. Chem. Rev. 1996, 96, 2097 and references therein.
2. 1 Alder, R.W. Acc. Chem. Res. 1983, 16, 321; Tetrahedron 1990, 46, 683; Alder, R.W. ; East, S. P. Chem. Rev. 1996, 96, 2097 and references therein.
3. 1 Alder, R.W. Acc. Chem. Res. 1983, 16, 321; Tetrahedron 1990, 46, 683; Alder, R.W. ; East, S. P. Chem. Rev. 1996, 96, 2097 and references therein.
4. 2 Gleiter, R.; Hövermann, K.; Ritter, J; Nuber, B. Angew. Chem. Int. Ed. Engl. 1995, 34, 789.
5. 3 Gleiter, R.; Wolfart, V. Tetrahedron Lett. 1996, 37, 479.
6. 4 Walls, L. P. Brit. Pat. 803 072, 1958; Chem. Abstr. 1958, 53: P 12242i.
7. 4 Walls, L. P. Brit. Pat. 803 072, 1958; Chem. Abstr. 1958, 53: P 12242i.
8. 5 Johnson, A. W. J. Chem. Soc. 1946, 1009.
9. 2: calcd. 240.1543, found 240.1585.
10. 1 = 0.046 (only for observed reflections), wR = 0.127.
11. 8 Burla, M. C.; Camalli, M.; Cascarano, G.; Giacovazzo, C.; Polidori, G.; Spagna, R.; Viterbo, D. J. Appl. Cryst. 22, 1989, 389-393. Details of the crystal structure determinations of 2 and 3 may be obtained from the Cambridge Crystallographic Data Center, University Chemical Laboratory, Lensfield Road, Cambridge CB21EW (UK) on quoting the full journal citation.
12. 9 Fair, C. K. An Interaktive Intelligent System for Crystal Structure Analysis, User Manual, Enraf - Nonius, Delft, The Netherlands. 1990.
13. 10 CRYSTAL STRUCTURE REFINEMENT, UNIX VERSION, Copyright(C) George M. Sheldrick 1993-7 Release 97-1.