Solvent free oxidation of β,β-disubstituted enamines under microwave irradiation

Tetrahedron Letters

Volumn 39, Issue 7, 1998, Pages 541-542

  Benhaliliba, Hadj ^b   Derdour, Aïcha ^b   Bazureau, Jean Pierre ^a   Texier Boullet, Françoise ^a   Hamelin, Jack ^a  

^a CNRS   (France)

^b NONE

Author keywords

[No Author keywords available]

Indexed keywords

ENAMINE; FORMAMIDE DERIVATIVE; KETONE DERIVATIVE; SOLVENT;

ARTICLE; MICROWAVE IRRADIATION; OXIDATION;

EID: 0032510015     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)10623-2     Document Type: Article

References (13)

1. 1. Harris, C.E. ; Lee, L.Y. ; Dorr, H. ; Singaram, B. Tetrahedron Lett., 1995, 36, 2921-2924 and references cited.
2. 2. Laurent, A. ; Jacquault, P. ; Di Martino, J.L. ; Hamelin, J. J.C.S. Chem. Commun., 1995, 1101. Jolivet, S. ; Abdallah-El Ayoubi, S. ; Mathé, D. ; Texier-Boullet, F. ; Hamelin, J. J. Chem. Res.(S), 1996, 300-301. Kerneur, G. ; Lerestif, J.M. ; Bazureau, J.P. ; Hamelin, J. Synthesis, 1997, 287-289. Michaud, D. ; Abdallah-El Ayoubi, S. ; Dozias, M.J. ; Toupet, L. ; Texier-Boullet, F. ; Hamelin, J. J.C.S. Chem. Commun., 1997, 1613-1614.
3. 2. Laurent, A. ; Jacquault, P. ; Di Martino, J.L. ; Hamelin, J. J.C.S. Chem. Commun., 1995, 1101. Jolivet, S. ; Abdallah-El Ayoubi, S. ; Mathé, D. ; Texier-Boullet, F. ; Hamelin, J. J. Chem. Res.(S), 1996, 300-301. Kerneur, G. ; Lerestif, J.M. ; Bazureau, J.P. ; Hamelin, J. Synthesis, 1997, 287-289. Michaud, D. ; Abdallah-El Ayoubi, S. ; Dozias, M.J. ; Toupet, L. ; Texier-Boullet, F. ; Hamelin, J. J.C.S. Chem. Commun., 1997, 1613-1614.
4. 2. Laurent, A. ; Jacquault, P. ; Di Martino, J.L. ; Hamelin, J. J.C.S. Chem. Commun., 1995, 1101. Jolivet, S. ; Abdallah-El Ayoubi, S. ; Mathé, D. ; Texier-Boullet, F. ; Hamelin, J. J. Chem. Res.(S), 1996, 300-301. Kerneur, G. ; Lerestif, J.M. ; Bazureau, J.P. ; Hamelin, J. Synthesis, 1997, 287-289. Michaud, D. ; Abdallah-El Ayoubi, S. ; Dozias, M.J. ; Toupet, L. ; Texier-Boullet, F. ; Hamelin, J. J.C.S. Chem. Commun., 1997, 1613-1614.
5. 2. Laurent, A. ; Jacquault, P. ; Di Martino, J.L. ; Hamelin, J. J.C.S. Chem. Commun., 1995, 1101. Jolivet, S. ; Abdallah-El Ayoubi, S. ; Mathé, D. ; Texier-Boullet, F. ; Hamelin, J. J. Chem. Res.(S), 1996, 300-301. Kerneur, G. ; Lerestif, J.M. ; Bazureau, J.P. ; Hamelin, J. Synthesis, 1997, 287-289. Michaud, D. ; Abdallah-El Ayoubi, S. ; Dozias, M.J. ; Toupet, L. ; Texier-Boullet, F. ; Hamelin, J. J.C.S. Chem. Commun., 1997, 1613-1614.
6. 3. Martinez, L.A. ; Garcia, O. Tetrahedron Lett., 1993, 34, 5293-5294.
7. 4. Delgado, F. ; Alvarez, C. ; Garcia, O. ; Penieres, G. ; Marquez, C. Synth. Commun., 1991, 21, 2137-2141.
8. 5. Delgado, F. ; Alvarez, C. ; Garcia, O. ; Medina, S. ; Marquez, C. Synth. Commun., 1991, 21, 619-624.
9. 6. Delgado, F. ; Garcia, O. Tetrahedron Lett., 1993, 34, 623-625.
10. 7. Harris, C.E. ; Chrisman, W. ; Bickford, S.A. ; Lee, L.Y. ; Torreblanca, A.E. ; Singaram, B. Tetrahedron Lett., 1997, 38, 981-984.
11. 8. One of the referees brought to our attention a very recent paper with analogous conclusions for the oxidation of arenes in the same conditions. Oussaid, A. ; Loupy, A. J. Chem. Res(S), 1997, 342-343.
12. 9. Commarnot, R. ; Diderot, R. ; Gardais, J.F. Fr. Demande 2, 560, 529 (Cl. B01J19/12), 06 Sept. 1985, Appl. 84/3, 496, 02 Mar 1984 ; Chem. Abstr. 1986, 105, 17442e. Apparatus commercialized by Prolabo (France) under the name Synthewave® 402. Temperature measured by an IR Captor : Prolabo. Patent 62241D, 1466 Fr, 23 Dec. 1991.
13. 9. Commarnot, R. ; Diderot, R. ; Gardais, J.F. Fr. Demande 2, 560, 529 (Cl. B01J19/12), 06 Sept. 1985, Appl. 84/3, 496, 02 Mar 1984 ; Chem. Abstr. 1986, 105, 17442e. Apparatus commercialized by Prolabo (France) under the name Synthewave® 402. Temperature measured by an IR Captor : Prolabo. Patent 62241D, 1466 Fr, 23 Dec. 1991.