Sonogashira cross-couplings using biocompatible conditions in water

Tetrahedron Letters

Volumn 39, Issue 7, 1998, Pages 525-528

  Dibowski, Harald ^a   Schmidtchen, Franz P ^a  

^a TECHNICAL UNIVERSITY OF MUNICH   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

ALKYNE DERIVATIVE; PHOSPHINE DERIVATIVE; POLYCYCLIC AROMATIC HYDROCARBON DERIVATIVE; PROTEIN;

AQUEOUS SOLUTION; ARTICLE; COVALENT BOND;

EID: 0032510011     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)10674-8     Document Type: Article

References (17)

1. th ICOS Conference, Amsterdam, June 1996.
2. 2) a) Review: Rossi, R., Carpita, A., Bellina, F., Org. Prep. Proced. Int. 1995, 27, 127-160;
3. b) Crisp, G. T., Flynn, B. L. J. Org. Chem. 1993, 58, 6614-6619;
4. c) Crisp, G. T., Gore, J. Tetrahedron 1997, 53, 1523 - 1544; idem. ibid. 1997, 53, 1505-1522;
5. c) Crisp, G. T., Gore, J. Tetrahedron 1997, 53, 1523 - 1544; idem. ibid. 1997, 53, 1505-1522;
6. d) Robins, M. J., Vinayak, R. S., Wood, S. G. Tetrahedron Lett. 1990, 31, 3731-3734.
7. 3) a) Casalnuovo, A. L., Calabrese, J. C., J. Am. Chem. Soc. 1990, 112, 4324-4330;
8. b) Bumagin, N. A., Sukhomlinova, L. I., Luzikova, E. V., Tolstaya, P. P., Beletskaya, I. P., Tetrahedron Lett. 1996, 37, 897-900;
9. c) Nguefack, J.-F., Bolitt, V., Sinou, D. Tetrahedron Lett. 1996, 37, 5527-5530.
10. 4) a) Dibowski, H., Schmidtchen, F.-P., Tetrahedron 1995, 57, 2325-2330;
11. b) Heßler, A., Stelzer, O., Sheldrick, W. S., Dibowski, H., Schmidtchen, F.P., J. Org. Chem. 1997, 62, 2362-2369.
12. 5) a) Cornils, B., Herrmann, W. A., Eckl, R. W., J. Molec. Catal A 1997, 116, 27-33;
13. b) Joó, F., Kathó, A., J. Molec. Catal. A 1997, 116, 3-26.
14. 2 and 5eq of the guanidino phosphine ligand chloride in water (0.01 M Pd). The mixture was kept at 4°C for 5 days. Within this period the catalytic activity gradually stabilised and then remained constant over several weeks.
15. 7) Doctoral dissertation B. Linow, TU München, 1995, to be published.
16. 8) Rudnik, D. A., McWherter, C. A., Gokel, G. W., Gordon, J. I. Adv. Enzymol. Rel. Areas Vol 67, 375-430 (1993).
17. 9) Kishore, N.S., Lu, T., Knoll, L.J., Katoh, A., Rudnik, D.A., Mehta, P.P., Devados, B., Huhn, M., Atwood, J.L., Adams, S.P., Gokel, G.W., Gordon, J.I. J.Biol.Chem. 1991, 266, 8835-8855.