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In addition to lactone 6, 4-phenylbutyrolactone was detected in runs 3, 4, 7, 8 in small amounts (<1%) by GC-MS spectrometry
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In addition to lactone 6, 4-phenylbutyrolactone was detected in runs 3, 4, 7, 8 in small amounts (<1%) by GC-MS spectrometry.
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26
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84889175064
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note
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3), would give a carbocation precursor of compound 2; (ii) 13 can be transformed to 14 via an intramolecular disproportionation. The collapse of 14 would lead to the formation of 4 and a "lead(I)" species.
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