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4. 8 (19g, 95%) was obtained after solvent removal and used in the next reaction without purification.
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34
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0010446240
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note
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13. Thioglycoside formation is probably occurred before debenzylation since the former reaction normally proceeds relatively fast as reported in ref. 5 d). The modest yields of 1a, b are likely due to cleavage of the formyl protecting group.
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Jain, R.K.1
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