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w=0.0426, GOF=1.573, max/min residual electron density=0.457/-0.330. Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre, as supplementary publications no. CCDC-101597 and 101598. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge, CB2 1EZ. (fax:(+44)1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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