Regio-selective bromination of multiflorine and structures of 3-bromomultiflorine and its molecular complex with succinimide

Journal of Molecular Structure

Volumn 442, Issue 1-3, 1998, Pages 103-113

  Borowiak, Teresa ^a   Kubicki, Maciej ^a   Wysocka, Waleria ^a   Przybył, Anna ^a  

^a ADAM MICKIEWICZ UNIVERSITY   (Poland)

Author keywords

Conformation in solution and in solid state; Lupine alkaloids; Multifiofine; Regio specific bromination; X ray crystal structure

Indexed keywords

EID: 0032477896     PISSN: 00222860     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-2860(97)00332-3     Document Type: Article

References (21)

1. [1] W. Wysocka, T. Brukwicki, Planta Med. 54 (1988) 522.
2. [2] I. Murakoshi, Y. Fujii, S. Takeda and I. Arai. Jpn. Kokai Tokkyo Koho JP No. 04, 295, 480 [92, 295, 480] (Cl. C07D471/18), 20 Oct 1992, Appl. 91/81,332; Mar 1991; 7 pp.
3. [3] M.H. Mohamed, A.-N.A. El-Shorbagi, J. Nat. Prod. 56 (1993) 1999.
4. [4] I. Jirkovsky, Can. J. Chem. 52 (1974) 55.
5. [5] D.L. Comins, P.J. Sajan, X. Chen, Tetrahedron Lett. 36 (1995) 9141.
6. [6] R. Munier, M. Macheboeuf, Bull. Soc. Chim. Biol. 33 (1951) 846.
7. [7] (a) W. Wysocka and T. Brukwicki, J. Mol. Stuct. 265 (1992) 143.
8. (b) W. Wysocka and T. Brukwicki, J. Mol. Struct. 385 (1996) 23.
9. [8] Kuma KM4 Software. User's Guide. Version 5.0. Kuma Diffraction, Wrocław, Poland, 1991.
10. [9] A.C.T. North, D.C. Phillips, F.S. Mathews, Acta Crystallogr. Sect. A: Found. Crystallogr. A24 (1968) 351.
11. [10] G.M. Sheldrick, Acta Crystallogr. Sect. A: Found. Crystallogr. A46 (1990) 467.
12. [11] G.M. Sheldrick, SHELXL93, Program for Crystal Structure Refinement, University of Göttingen, Germany, 1993.
13. [12] M. Kubicki, T. Borowiak, Acta Crystallogr. Sect. C: Cryst. Struct. Commun. C45 (1989) 1047.
14. [13] S. Okuda, H. Kataoka, T. Tsuda, Chem. Pharm. Bull. 13 (1965) 487.
15. [14] S. Klyne, P.N. Scopes, R.N. Thomas, J. Skolik, J. Gawroński, M. Wiewiórowski, J. Chem. Soc. Perkin Trans. 1 (1974) 2565.
16. [15] D. Pyźalska, M. Gdaniec, T. Borowiak, J. Wolińska-Mocydlarz, Acta Crystallogr. Sect. B: Structural Science B36 (1980) 1602.
17. [16] W.L. Duax and D.A. Norton, Atlas of Steroid Structure, Plenum Press, New York, 1975, pp. 16-22.
18. [17] T. Borowiak, I. Wolska, J. Mol. Struct. 374 (1996) 97.
19. [18] E.L. Eliel, Chem. Ind. (London), (1959) 568.
20. [19] C.A.G. Haasnoot, F.A.A.H. de Leeuw, C. Altona, Tetrahedron 36 (1980) 2783.
21. [20] Stereochemical Workstation Operation Manual, Release 3.4. Siemens Analytical X-Ray Instruments Inc., Madison, Wisconsin, USA, 1989.