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note
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13I: C, 33.79%, H, 3.25%, Found: C, 33.63%, H, 2.98%.
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24
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0010463833
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note
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3, 300 MHz). 1b: 4.48-4.27 (3 H, m), 3.00-2.68 (2 H, m); 2b: 5.30 (1 H, m), 4.52-4.10 (3 H, m), 3.20 (1 H, dd, J = 5.0, 10.5 Hz), 3.01-2.68 (3 H, m); 3b: 4.44-4.25 (3 H, m), 3.62 (1 H, m), 3.00-2.68 (2 H, m); 4b: 6.30 (0.3 H, d, J = 3.5 Hz), 5.63 (0.3 H, dd, J = 1.8, 8.2 Hz), 5.20-5.00 (1.7 H, m), 4.37-3.68 (7.7 H, m), 3.05-2.81 (1 H, m), 2.73-2.50 (1 H, m), 2.18-2.00 (12 H, m); 5b: 5.11 (1 H, s), 4.40 (1 H, m), 4.16-3.98 (4 H, m), 3.85, 3.76 (0.5 H each, dd each), 3.20-2.95 (2 H, m), 2.72-2.46 (3 H, m); 6b: 5.55, 5.53 (0.5 H each, s each), 4.69 (1 H, m), 4.48-4.38 (3 H, m), 4.18-3.92 (4 H, m), 3.86-3.61 (3 H, m), 3.50-3.40 (2 H, m), 3.38-2.60 (4 H, m).
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26
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0010463240
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Dissertation, Shanghai Institute of Organic Chemistry
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