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85038544796
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note
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9 with modifications as follows: tert-butylmethylether for the extraction and the organic layer was drying over anhydrous calcium chloride. TBDMS formation was carried out at room temperature by adding 50 μ1 of isooctane and 50 μ1 of silylating agent to the evaporation residue.
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11
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85038554571
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note
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-1) and electron impact for ionization (70 ev; emission current, 0.2 mA).
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12
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85038538766
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note
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-1. Injector and detector temperatures: 250°C and 275°C, respectively.
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13
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2-oxo acid reductase ∼ 2-oxo carboxylate reductase ∼ 2-hydroxy acid dehydrogenase; E.C. 1.1.99.x; Academic Press: San Diego
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