Regioselective synthesis and properties of 3-cyano-6-methyl-4-trifluoromethylpyridine-2(1H)-thione. Molecular and crystal structure of 3-cyano-2-ethylthio-6-methyl-4-trifluoromethylpyridine

Russian Chemical Bulletin

Volumn 47, Issue 3, 1998, Pages 465-468

  Nikishin, K G ^a   Kislyi, V P ^a   Nesterov, V N ^b   Shestopalov, A M ^a   Struchkov, Yu T ^b   Semenov, V V ^a  

^a N D ZELINSKY INSTITUTE OF ORGANIC CHEMISTRY   (Russian Federation)

^b A N NESMEYANOV INSTITUTE OF ORGANOELEMENT COMPOUNDS   (Russian Federation)

Author keywords

3 aminothieno 2,3 b pyridines; 3 cyano 2 ethylthio 6 methyl 4 trifluoromethylpyridine; 3 cyano 6 methyl 4 trifluoromethylpyridine 2(1H) thione; Cyanothioacetamide; X ray diffraction analysis

Indexed keywords

EID: 0032386004     PISSN: 10665285     EISSN: None     Source Type: Journal    
DOI: 10.1007/BF02495655     Document Type: Article

References (15)

1. V. P. Litvinov, L. A. Rodinovskaya, Yu. A. Sharanin, A. M. Shestopalov, and A. Senning, Sulfur Reports, 1992, 13, 155.
2. L. A. Rodinovskaya, Dr. Sc. (Chem.) Thesis, N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences, Moscow, 1994 (in Russian).
3. B. Iddon, H. Suschitzky, A. W. Thompson, and E. Ager, J. Chem. Soc., Perkin Trans, 1, 1974, 2300.
4. S. Portnoy, J. Org. Chem., 1965, 30, 3377.
5. L. A. Rodinovskaya, Yu. A. Sharanin, V. P. Litvinov, A. M. Shestopalov, V. K. Promonenkov, B. M. Zolotarev, and V. Yu. Mortikov, Zh. Org. Khim., 1985, 21, 2439 [J. Org. Chem. USSR, 1985, 21 (Engl. Transl.)].
6. L. A. Rodinovskaya, Yu. A. Sharanin, V. P. Litvinov, A. M. Shestopalov, V. K. Promonenkov, B. M. Zolotarev, and V. Yu. Mortikov, Zh. Org. Khim., 1985, 21, 2439 [J. Org. Chem. USSR, 1985, 21 (Engl. Transl.)].
7. F. H. Allen, O. Kennard, D. G. Watson, L. Brammer, A. G. Orpen, and R. Taylor, J. Chem. Soc., Perkin Trans. 2, 1987, 1.
8. .A. Bondi, J. Phys. Chem., 1966, 70, 3006.
9. V. P. Litvinov, E. E. Apenova, Yu. A. Sharanin, V. P. Nesterov, V. E. Shklover, and Yu. T. Struchkov, Izv. Akad. Nauk SSSR, Ser. Khim., 1986, 145 [Bull. Acad. Sci. USSR, Div. Chem. Sci., 1986, 35, 131 (Engl. Transl.)].
10. V. P. Litvinov, E. E. Apenova, Yu. A. Sharanin, V. P. Nesterov, V. E. Shklover, and Yu. T. Struchkov, Izv. Akad. Nauk SSSR, Ser. Khim., 1986, 145 [Bull. Acad. Sci. USSR, Div. Chem. Sci., 1986, 35, 131 (Engl. Transl.)].
11. V. N. Nesterov, L. A. Rodinovskaya, V. P. Litvinov, Yu. A. Sharanin, A. M. Shestopalov, V. Yu. Mortikov, V. I. Shvedov, V. E. Shklover, and Yu. T. Struchkov, Izv. Akad. Nauk SSSR, Ser. Khim., 1988, 140 [Bull. Acad. Sci. USSR, Div. Chem. Sci., 1988, 37, 129 (Engl. Transl.)].
12. V. N. Nesterov, L. A. Rodinovskaya, V. P. Litvinov, Yu. A. Sharanin, A. M. Shestopalov, V. Yu. Mortikov, V. I. Shvedov, V. E. Shklover, and Yu. T. Struchkov, Izv. Akad. Nauk SSSR, Ser. Khim., 1988, 140 [Bull. Acad. Sci. USSR, Div. Chem. Sci., 1988, 37, 129 (Engl. Transl.)].
13. V. N. Nesterov, V. E. Shklover, Yu. T. Struchkov, Yu. A. Sharanin, M. P. Goncharenko, and V. D. Dyachenko, Izv. Akad. Nauk SSSR, Ser. Khim., 1991, 521 [Bull. Acad. Sci. USSR, Div. Chem. Sci., 40, 453 (Engl. Transl.)].
14. V. N. Nesterov, V. E. Shklover, Yu. T. Struchkov, Yu. A. Sharanin, M. P. Goncharenko, and V. D. Dyachenko, Izv. Akad. Nauk SSSR, Ser. Khim., 1991, 521 [Bull. Acad. Sci. USSR, Div. Chem. Sci., 40, 453 (Engl. Transl.)].
15. W. Robinson, in: Crystallographic Computing - Techniques and New Technologies, Oxford Univ. Press, Oxford, 1988, 366.