Synthesis of a silylene-and hydride-bridged Re-W heterobimetallic complex and its photolysis to form novel silenyl-bridged heterobimetallic complexes

Chemistry Letters

Volumn , Issue 2, 1998, Pages 149-150

  Sakaba, Hiroyuki ^a   Ishida, Kazushige ^a   Horino, Hiroshi ^a  

^a TOHOKU UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0032373585     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1998.149     Document Type: Article

References (24)

1. H. Sakaba, K. Ishida, and H. Horino, Chem. Lett., 1995, 1145.
2. J. Powell, J. F. Sawyer, and M. Shiralian, Organometallics, 8, 577 (1989).
3. 2RcSi 438.1025.
4. C. P. Casey, H. Sakaba, and T. L. Underiner, J. Am. Chem. Soc., 113, 6673 (1991).
5. D. F. Dong, J. K. Hoyano, and W. A. G. Graham, Can. J. Chem., 59, 1455 (1981).
6. 4ReSiW: C, 38.47; H, 4.59%.
7. For reviews, see: H. D. Kaesz and R. B. Saillant, Chem. Rev., 72, 231 (1972); D. S. Moore and S. D. Robinson, Chem. Soc. Rev., 12, 415 (1983).
8. For reviews, see: H. D. Kaesz and R. B. Saillant, Chem. Rev., 72, 231 (1972); D. S. Moore and S. D. Robinson, Chem. Soc. Rev., 12, 415 (1983).
9. +, 5).
10. 2ReSi 439.1087.
11. -1.
12. Y. Kawano, H. Tobita, and H. Ogino, J. Organomet. Chem., 428, 125 (1992) and references therein.
13. 1/2 = 5 Hz), but the small couplings were not seen for the WH signal.
14. 1H COSY spectrum at -60°C: δ -9.33 ↔ 0.92. -9.33 ↔ 1.39, -0.17 ↔ 1.39.
15. C. Lewis and M. S. Wrighton, J. Am. Chem. Soc., 105, 7768 (1983).
16. B. K. Campion, R. H. Heyn, T. D. Tilley, and A. L. Rheingold, J. Am. Chem. Soc., 115, 5527 (1993).
17. For recent reviews, see: A. G. Brook and M. A. Brook, Adv. Organomet. Chem., 39, 71 (1996); P. D. Lickiss, Chem. Soc. Rev., 21, 271 (1992).
18. For recent reviews, see: A. G. Brook and M. A. Brook, Adv. Organomet. Chem., 39, 71 (1996); P. D. Lickiss, Chem. Soc. Rev., 21, 271 (1992).
19. D. H. Berry and L. J. Procopio, J. Am. Chem. Soc., 111, 4099 (1989); A. A. Zlota, F. Frolow, and D. Milstein, J. Chem. Soc., Chem. Commun., 1989, 1826; H. Yamashita, A. M. Kawamoto, M. Tanaka, and M. Goto, Chem. Lett., 1990, 2107; P. I. Djurovich, P. J. Carroll, and D. H. Berry, Organometallics, 13, 2551 (1994); P. I. Djurovich, A. R. Dolich, and D. H. Berry, J. Chem. Soc., Chem. Commun., 1994, 1897; H. Yamashita and M. Tanaka, Bull. Chem. Soc. Jpn., 68, 403 (1995) and refereces therein.
20. D. H. Berry and L. J. Procopio, J. Am. Chem. Soc., 111, 4099 (1989); A. A. Zlota, F. Frolow, and D. Milstein, J. Chem. Soc., Chem. Commun., 1989, 1826; H. Yamashita, A. M. Kawamoto, M. Tanaka, and M. Goto, Chem. Lett., 1990, 2107; P. I. Djurovich, P. J. Carroll, and D. H. Berry, Organometallics, 13, 2551 (1994); P. I. Djurovich, A. R. Dolich, and D. H. Berry, J. Chem. Soc., Chem. Commun., 1994, 1897; H. Yamashita and M. Tanaka, Bull. Chem. Soc. Jpn., 68, 403 (1995) and refereces therein.
21. D. H. Berry and L. J. Procopio, J. Am. Chem. Soc., 111, 4099 (1989); A. A. Zlota, F. Frolow, and D. Milstein, J. Chem. Soc., Chem. Commun., 1989, 1826; H. Yamashita, A. M. Kawamoto, M. Tanaka, and M. Goto, Chem. Lett., 1990, 2107; P. I. Djurovich, P. J. Carroll, and D. H. Berry, Organometallics, 13, 2551 (1994); P. I. Djurovich, A. R. Dolich, and D. H. Berry, J. Chem. Soc., Chem. Commun., 1994, 1897; H. Yamashita and M. Tanaka, Bull. Chem. Soc. Jpn., 68, 403 (1995) and refereces therein.
22. D. H. Berry and L. J. Procopio, J. Am. Chem. Soc., 111, 4099 (1989); A. A. Zlota, F. Frolow, and D. Milstein, J. Chem. Soc., Chem. Commun., 1989, 1826; H. Yamashita, A. M. Kawamoto, M. Tanaka, and M. Goto, Chem. Lett., 1990, 2107; P. I. Djurovich, P. J. Carroll, and D. H. Berry, Organometallics, 13, 2551 (1994); P. I. Djurovich, A. R. Dolich, and D. H. Berry, J. Chem. Soc., Chem. Commun., 1994, 1897; H. Yamashita and M. Tanaka, Bull. Chem. Soc. Jpn., 68, 403 (1995) and refereces therein.
23. D. H. Berry and L. J. Procopio, J. Am. Chem. Soc., 111, 4099 (1989); A. A. Zlota, F. Frolow, and D. Milstein, J. Chem. Soc., Chem. Commun., 1989, 1826; H. Yamashita, A. M. Kawamoto, M. Tanaka, and M. Goto, Chem. Lett., 1990, 2107; P. I. Djurovich, P. J. Carroll, and D. H. Berry, Organometallics, 13, 2551 (1994); P. I. Djurovich, A. R. Dolich, and D. H. Berry, J. Chem. Soc., Chem. Commun., 1994, 1897; H. Yamashita and M. Tanaka, Bull. Chem. Soc. Jpn., 68, 403 (1995) and refereces therein.
24. D. H. Berry and L. J. Procopio, J. Am. Chem. Soc., 111, 4099 (1989); A. A. Zlota, F. Frolow, and D. Milstein, J. Chem. Soc., Chem. Commun., 1989, 1826; H. Yamashita, A. M. Kawamoto, M. Tanaka, and M. Goto, Chem. Lett., 1990, 2107; P. I. Djurovich, P. J. Carroll, and D. H. Berry, Organometallics, 13, 2551 (1994); P. I. Djurovich, A. R. Dolich, and D. H. Berry, J. Chem. Soc., Chem. Commun., 1994, 1897; H. Yamashita and M. Tanaka, Bull. Chem. Soc. Jpn., 68, 403 (1995) and refereces therein.