Structure of 1,5-anhydro-D-fructose: X-ray analysis of crystalline acetylated dimeric forms

Journal of Carbohydrate Chemistry

Volumn 17, Issue 7, 1998, Pages 1027-1035

  Andersen, Søren M ^a   Lundt, Inge ^a   Marcussen, Jan ^b   Sotofte I ^a   Yu, Shukun ^b  

^a TECHNICAL UNIVERSITY OF DENMARK   (Denmark)

^b DANISCO A S   (Denmark)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0032333831     PISSN: 07328303     EISSN: None     Source Type: Journal    
DOI: 10.1080/07328309808001881     Document Type: Article

References (18)

1. th European Carbohydrate Symposium, Utrecht, Netherlands, July 6-11, 1997, Poster A138.
2. F. W. Lichtenthaler, E. S. H. El Ashry, and V. H. Göckel, Tetrahedron Lett., 21, 1429 (1980).
3. G. Deffieux, R. Baute, M.-A. Baute, M. Atfani, and A. Carpy, Phytochemistry, 26, 1391 (1987).
4. S. Yu and M. Pedersén, Planta, 191, 137 (1993).
5. S. Yu, L. Kenne, and M Pedersén, Biochim. Biophys. Acta, 1156, 313 (1993).
6. S. Yu, T. Ahmad, L. Kenne, and M. Pedersén, Biochim. Biophys. Acta, 1244, 1 (1995).
7. S. Kametani, H. Mizuno, Y. Shiga, and H. Akanuma, J. Biochem., 119, 180 (1996).
8. T. Nakamura, A. Naito, Y. Takahashi, and H. Akanuma, J. Biochem., 99, 607 (1986).
9. M. Suzuki, S. Kametani, K. Uchida, and H. Akanuma, Eur. J. Biochem., 240, 23 (1996).
10. T. Nakamura, A. Takahashi, and K. Kato, Jpn. Patent Application, Chem. Abstr., 109, 110835 (1988).
11. a) S. Yu, K. Bojsen, and J. Marcussen, Int. Patent Application, Chem. Abstr., 125, 56375 (1996).
12. b) S. Yu, K. Bojsen, K. M. Kragh, M. Bojko, J. Nielsen, J. Marcussen, and T. M. I. E. Christensen, Int. Patent Application, Chem. Abstr., 123, 226024 (1995).
13. T. Taguchi, M. Haruna and J. Okuda, Biotechnol. Appl. Biochem., 18, 275 (1993).
14. max = 50°. The structure was solved by direct methods (SHELXTL) and refined with full matrix least-squares giving R = 0.1280 [2475 refl., I > 2σ(I)] and wR2 = 0.3354 (4710 refl.). The quality and the reflecting power of the crystals were rather poor. Tables of atomic coordinates, bond lengths, and bond angles have been deposited with the Cambridge Crystallographic Data Center. These tables may be obtained on request from the Director, Cambridge Crystallographic Data Center, 12 Union Road, Cambridge CB2 IEZ, UK.
15. M. Brehm, W.G. Dauben, P. Köhler, and F.W. Lichtenthaler, Angew. Chem., 99, 1318 (1987) (Int. Ed. Engl. 26, 1271 (1987)).
16. M. Brehm, W.G. Dauben, P. Köhler, and F.W. Lichtenthaler, Angew. Chem., 99, 1318 (1987) (Int. Ed. Engl. 26, 1271 (1987)).
17. P. Jarglis and F.W. Lichtenthaler, Angew. Chem., 94, 140 (1982) (Int. Ed. Engl. 21, 141 (1982)).
18. P. Jarglis and F.W. Lichtenthaler, Angew. Chem., 94, 140 (1982) (Int. Ed. Engl. 21, 141 (1982)).