NMR spectroscopy of 13C-enriched polysaccharides: Application of 13C-13C TOCSY to sugars of different configuration

Magnetic Resonance in Chemistry

Volumn 36, Issue 2, 1998, Pages 128-131

  Kjellberg, Alexandra ^a   Nishida, Toshiaki ^b   Weintraub, Andrej ^c   Widmalm, Göran ^a  

^a STOCKHOLM UNIVERSITY   (Sweden)

^b Box 17035   (Sweden)

^c KAROLINSKA INSTITUTE   (Sweden)

Author keywords

13C NMR; Lipopolysaccharide; NMR; Saccharide; TOCSY

Indexed keywords

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POLYSACCHARIDES;

13C NMR; BACTERIAL POLYSACCHARIDES; CARBON-13; COHERENCE TRANSFER; GALACTO-CONFIGURATIONS; LIPOPOLYSACCHARIDES; NMR-SPECTROSCOPY; PROTON DETECTIONS; SACCHARIDE; TOCSY;

SUGARS;

EID: 0032331247     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1097-458X(199802)36:2<128::AID-OMR226>3.0.CO;2-L     Document Type: Article

References (23)

1. U. Piantini, O. W. Sørensen and R. R. Ernst, J. Am. Chem. Soc. 104, 6800 (1982).
2. L. Braunschweiler and R. R. Ernst, J. Magn. Reson. 53, 521 (1983).
3. V. Wray, Prog. Nucl. Magn. Reson. Spectrosc. 13, 177 (1979).
4. M. J. King-Morris and A. S. Serianni, J. Am. Chem. Soc. 109, 3501 (1987).
5. J. Wu, P. B. Bondo, T. Vourinen and A.S. Serianni, J. Am. Chem. Soc. 114, 3499 (1992).
6. G. M. Clore and A. M. Gronenborn, Methods Enzymol 239, 349 (1994).
7. A. Pardi, Methods Enzymol. 261, 350 (1995).
8. V. Bossennec, F. P. B. Perly and P. Berthault, J. Magn. Reson. 28, 149 (1990).
9. L. Yu, R. Goldman, P. Sullivan, G. F. Walker and S. W. Fesik, J. Biomol. NMR 3, 429 (1993).
10. J. Chung, J. R. Tolman, K. P. Howard and J. H. Prestegard, J. Magn. Reson. 102B, 137 (1993).
11. R. Harris, T. J. Rutherford, M. J. Milton and S. W. Homans, J. Biomol NMR 9, 47 (1997).
12. D. N. M. Jones and J. K. M. Sanders, J. Am. Chem. Soc. 111, 5132 (1989).
13. D. N. M. Jones and J. K. M. Sanders, J. Chem. Soc., Chem. Commun. 167 (1989).
14. Q. Wu and C. A. Bush, Biochemistry 35, 14512 (1996).
15. Q. Xu and C. A. Bush, Biochemistry 35, 14521 (1996).
16. L. Kenne, B. Lindberg, J. K. Madden, A. A. Lindberg and J. P. Gemski, Carbohydr. Res. 122, 249 (1983).
17. D. J. Harvey, J. Chromatogr. A 720, 429 (1996).
18. V. N. Shibaev, Adv. Carbohydr. Chem. Biochem. 44, 277 (1986).
19. A. Bax and D. G. Davis, J. Magn. Reson. 65, 355 (1985).
20. A. Bax, G. M. Clore and A. M. Gronenborn, J. Magn. Reson. 88, 425 (1990).
21. L. E. Kay, G.-Y. Xu, A. U. Singer, D. R. Muhandiram and J. D. Forman-Kay, J. Magn. Reson. B 101, 333 (1993).
22. O. Westphal, O. Lüderitz and F. Bister, Z. Naturforsch, 7, 148 (1952).
23. A. J. Shaka, C. J. Lee and A. Pines, J. Magn. Reson. 77, 274 (1988).