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The phenylthioglycoside derived from the 3-Omethyl-4-O-benzyl analog of 3, as well as its sulfoxide, did not couple with 2c in satisfactory yield
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The phenylthioglycoside derived from the 3-Omethyl-4-O-benzyl analog of 3, as well as its sulfoxide, did not couple with 2c in satisfactory yield.
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2 was titrated to a colorless endpoint with aqueous sodium thiosulfate (0.005M)
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2 was titrated to a colorless endpoint with aqueous sodium thiosulfate (0.005M).
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