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13
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0042837278
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note
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8Sm: C, 49.92; H, 4.97%.
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14
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0041334577
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note
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-1= 14.83, Temp= -80 °C, Rf/Rw= 0.048/0.049, GOF= 1.52. No. of unique reflections= 10986.
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15
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0041161999
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19
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0042336393
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One THF molecule was removed by drying in vacuo
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One THF molecule was removed by drying in vacuo.
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20
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23
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0041334573
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note
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3), 120.3, 124.4, 129.0, 129.3, 129.4, 132.1, 138.1, 142.3, (Ar), 165.8 (NHCO), 188.7 (COS).
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24
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0041334574
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