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11544367026
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note
-
A detailed paper concerning the eletrochemical stability of self assembled monolayers, related to the way of attachment (thiol versus sulfide) and number of attachment points, is in preparation.
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16
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11544290617
-
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note
-
The use of sulfur nucleophiles would lead to the formation of sulfides connecting the dialkylsulfides to the cyclodextrin, resulting in two sets of chemically equivalent dialkyl sulfides and an undesired competition for binding on the gold surface.
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34
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0026034127
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Ashton, P. R.; Ellwood, P.; Staton, J.; Stoddart, J. F. Angew. Chem., Int. Ed. Engl. 1991, 30, 80-81.
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11544304649
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The Chemistry of Thioethers: Difference and Analogies with Ethers
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Patai, S., Ed.; New York.
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Brandsma, L.1
Arens, J.F.2
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36
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11544290616
-
-
For a review see (a) Klausner, Y. S.; Bodansky, M. Synthesis 1972, 53-463. (b) Haslam E. Tetrahedron 1980, 36, 2409-2433.
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Klausner, Y.S.1
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33745361073
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For a review see (a) Klausner, Y. S.; Bodansky, M. Synthesis 1972, 53-463. (b) Haslam E. Tetrahedron 1980, 36, 2409-2433.
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Haslam, E.1
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38
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11544360662
-
-
3-(Thiomethyl) propionic acid (5) was prepared by basic hydrolysis of the commercially available methyl-3-methylthiopropionater: Corey, E. J.; Stékely, I.; Shiner, C. H. Tetahedron Letl. 1977, 3529-3532.
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Corey, E.J.1
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-
39
-
-
11544323783
-
-
12-(Thiododectly)dodecanoic acid (8) was synthesited according to literature procedures (ref 3a)
-
12-(Thiododectly)dodecanoic acid (8) was synthesited according to literature procedures (ref 3a).
-
-
-
-
40
-
-
1842442545
-
-
Sheehan, J. C.; Crickshank, P. A.; Boshart, G. L. J. Org. Chem. 1961, 26, 2525-2529.
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-
-
11544278230
-
-
note
-
-1). These measurements indicate that, for the preparation of monolayers using molecules which are attached to the surface via multiple points of attachment, the direct adsorption process is superior to an in situ preparation. The reactions of further amine functionalities of an already attached cyclodextrin molecule with the activated surface is apparently not favored, leaving a large amount of unreacted activated ester even after "completion" of the surface reaction.
-
-
-
-
43
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0342459190
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85085632101
-
-
note
-
shortthiol (11:1/ 10:1).
-
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45
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33845281250
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0001293239
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(c) Castner, D. G.; Hinds, K.; Grainger, D. W. Langmuir 1996, 12, 5083-5086.
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-
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85085632438
-
-
note
-
2p1/2) to determine the ratio between bound and unbound sulfur.
-
-
-
-
51
-
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7044264879
-
-
Beulen, M. W. J.; Huisman, B.-H.; van der Heijden, P. A.; van Veggel, F. C. J. M. Simons, M. G.; Biemond, E. M. E. F.; de Lange, P. J.; Reinhoudt, D. N. Langmuir 1996, 12, 6170-6172.
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52
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11544293350
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Negative TOF-SIMS spectra mainly exhibit sulfur-gold clusters
-
Negative TOF-SIMS spectra mainly exhibit sulfur-gold clusters.
-
-
-
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