Effects of sample preparation conditions on biomolecular solid-state NMR lineshapes

Journal of Biomolecular NMR

Volumn 12, Issue 3, 1998, Pages 417-421

  Jakeman, David L ^a   Mitchell, Dan J ^a   Shuttleworth, Wendy A ^a   Evans, Jeremy N S ^a  

^a WASHINGTON STATE UNIVERSITY   (United States)

Author keywords

31P NMR; EPSP synthase; Fast freezing; Narrowing linewidths; Solid state nmr; Trehalose

Indexed keywords

3 PHOSPHOSHIKIMATE 1 CARBOXYVINYLTRANSFERASE; BACTERIAL PROTEIN; DRUG DERIVATIVE; GLYCINE; GLYPHOSATE; MACROGOL DERIVATIVE; SHIKIMIC ACID; SHIKIMIC ACID 3 PHOSPHATE; SHIKIMIC ACID-3-PHOSPHATE; TRANSFERASE; TREHALOSE;

ARTICLE; CHEMISTRY; COMPARATIVE STUDY; FREEZING; LABORATORY DIAGNOSIS; MACROMOLECULE; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

3-PHOSPHOSHIKIMATE 1-CARBOXYVINYLTRANSFERASE; ALKYL AND ARYL TRANSFERASES; BACTERIAL PROTEINS; FREEZING; GLYCINE; MACROMOLECULAR SUBSTANCES; MAGNETIC RESONANCE SPECTROSCOPY; POLYETHYLENE GLYCOLS; SHIKIMIC ACID; SPECIMEN HANDLING; TREHALOSE;

EID: 0032175923     PISSN: 09252738     EISSN: None     Source Type: Journal    
DOI: 10.1023/A:1008305118426     Document Type: Article

References (39)

1. Appleyard, R.J. and Evans, J.N.S. (1993) J. Magn. Reson. Series B, 102, 245-252.
2. Appleyard, R.J., Shuttleworth, W.A. and Evans, J.N. S. (1994) Biochemistry, 33, 6812-6821.
3. Barlow, P.N., Appleyard, R.J., Wilson, B.J.O. and Evans, J.N.S. (1989) Biochemistry, 28, 7985-7991 and correction p. 10093.
4. Bondinell, W.E., Vrek, J., Knowles, P.F., Sprecher, M. and Sprinson, D.B. (1971) J. Biol Chem., 246, 6191-6196.
5. Bradford, M.M. (1976) Anal. Biochem., 72, 248-254.
6. Butler, S.L. and Falke, J.J. (1996) Biochemistry, 35, 10595-10600.
7. Carpenter, J.F., Pikal, M.J., Chang, B.S. and Randolph, T.W. (1997) Pharm. Res., 14, 969-975.
8. Chen, P.S., Toribara, T.Y. and Warner, H. (1956) Anal. Chem., 28, 1756-1758.
9. Christensen, A.M. and Schaefer, J. (1993) Biochemistry, 32, 2868-2873.
10. Clegg, J.S. (1965) Comp. Biochem. Physiol., 14, 135-143.
11. Crowe, L.M., Reid, D.S. and Crowe, J.H. (1996) Biophys. J., 71, 2087-2093.
12. Evans, J.N.S. (1992) In Pulsed Magnetic Resonance: NMR, ESR and Optics (A Recognition of E.L. Hahn) Oxford University Press, Oxford and New York.
13. Evans, J.N.S. (1995) In Encyclopedia of NMR, John Wiley & Sons.
14. Evans, J.N.S. (1996) Biomolecular NMR Spectroscopy, Oxford University Press, Oxford and New York.
15. Evans, J.N.S., Appleyard, R.J. and Shuttleworth, W. (1992) Bull. Magn. Reson., 14, 81-85.
16. Evans, J.N.S., Appleyard, R.J. and Shuttleworth, W.A. (1993) J. Am. Chem. Soc., 115, 1588-1590.
17. Glaubitz, C. and Watts, A. (1998) J. Magn. Reson., 130, 305-316.
18. Gregory, R.B., Gangoda, M., Gilpin, R.K. and Su, W. (1993a) Biopolymers, 33, 1871-1876.
19. Gregory, R.B., Gangoda, M., Gilpin, R.K. and Su, W. (1993b) Biopolymers, 33, 513-519.
20. Griffiths, J.M. and Griffin, R.G. (1993) Anal. Chim. Acta, 283, 1081-1101.
21. Lazo, N.D., Hu, W. and Cross, T.A. (1992) J. Chem. Soc., Chem. Commun., 1529-1531.
22. Lazo, N.D., Hu, W., Lee, K.-C. and Cross, T.A. (1993) Biochem. Biophys. Res. Commun., 197, 904-909.
23. Lee, C.W., Das Gupta, S.K., Mattai, J., Shipley, G.G., Abdel-Mageed, O.H., Makriyannis, A. and Griffin, R.G. (1989) Biochemistry, 28, 5000-5009.
24. Lee, C.W., Waugh, J.S. and Griffin, R.G. (1986) Biochemistry, 25, 3737-3742.
25. Lin, T.Y. and Timasheff, S.N. (1996) Protein Sci., 5, 372-381.
26. McDowell, L.M., Klug, C.A., Beusen, D.D. and Schaefer, J. (1996a) Biochemistry, 35, 5395-5403.
27. McDowell, L.M. and Schaefer, J. (1996) Curr. Opin. Struct. Biol., 6, 624-629.
28. McDowell, L.M., Schmidt, A., Cohen, E.R., Studelska, D.R. and Schaefer, J. (1996b) J. Mol. Biol., 256, 160-171.
29. Millican, R.C. (1963) Anal Biochem., 6, 181.
30. Opella, S.J. (1997) Nat. Struct. Biol., 4, 845-848.
31. Shuttleworth, W.A., Hough, C.D., Bertrand, K.P. and Evans, J.N.S. (1992) Protein Eng., 5, 461-466.
32. Sikorski, J.A. and Gruys, K.J. (1997) Acc. Chem. Res., 30, 2-8.
33. Smith, S.O. and Peersen, O.B. (1992) Annu. Rev. Biophys. Biomol. Struct., 21, 25-47.
34. Tjandra, N. and Bax, A. (1997) Science, 278, 1697-1697.
35. Tomita, Y., Oconnor, E.J. and McDermott, A. (1994) J. Am. Chem. Soc., 116, 8766-8771.
36. Tycko, R. (1996) J. Biomol. NMR, 8, 239-251.
37. Van Veldhoven, P.P. and Mannaerts, G.P. (1987) Anal Biochem., 161, 45-48.
38. Xie, G. and Timasheff, S.N. (1997a) Protein Sci., 6, 211-221.
39. Xie, G. and Timasheff, S.N. (1997b) Biophys. Chem., 64, 25-43.