TEM/EELS characterization of a sintered polycrystalline silicon carbide fiber

Journal of the American Ceramic Society

Volumn 81, Issue 8, 1998, Pages 2037-2044

  Tenailleau, H ^a   Bourrat, Xavier ^a   Naslain, Roger ^a,d   Tressler, Richard E ^b,d   Giannuzzi, Lucille A ^c,d  

^a Laboratoire des Composites Thermostructuraux   (France)

^b PENNSYLVANIA STATE UNIVERSITY   (United States)

^c University of Central Florida   (United States)

^d AMERICAN CERAMIC SOCIETY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

BORON CARBIDE; CARBON; CRYSTAL STRUCTURE; ELECTRON ENERGY LOSS SPECTROSCOPY; GRAIN SIZE AND SHAPE; POLYCRYSTALLINE MATERIALS; POROUS MATERIALS; PRECIPITATION (CHEMICAL); SILICON CARBIDE; STOICHIOMETRY; TRANSMISSION ELECTRON MICROSCOPY;

TURBOSTRATIC CARBON;

CERAMIC FIBERS;

EID: 0032140384     PISSN: 00027820     EISSN: None     Source Type: Journal    
DOI: 10.1111/j.1151-2916.1998.tb02585.x     Document Type: Article

References (35)

1. S. Yajima, J. Hayashi, and M. Omori, "Continuous Silicon Carbide Fiber of High Tensile Strength," Chem. Lett., 931-34 (1975).
2. K. Okamura, "Ceramic Fibres from Polymer Precursors," Composites, 18 [2] 107-20 (1987).
3. C. Laffon, A. M. Flank, P. Lagarde, M. Laridjani, R. Hagege, P. Olry, J. Cotteret, J. Dixmier, J. L. Miquel, H. Hammel, and A. P. Legrand, "Study of Nicalon-Based Ceramic Fibres and Powders by EXAFS Spectrometry, X-ray Diffractometry and Some Additional Methods," J. Mater. Sci., 24, 1503-12 (1989).
4. L. Porte and A. Sartre, "Evidence for a Silicon Oxycarbide Phase in the Nicalon Silicon Carbide Fibre," J. Mater. Sci., 24, 271-75 (1989).
5. P. Le Costumer, M. Monthioux, and A. Oberlin, "Understanding Nicalon Fibre," J. Eur. Ceram. Soc., 11, 95-103 (1993).
6. R. Naslain, "Fibers from Organic/Organometallic Precursors"; in Advanced Inorganic Fibers. Edited by F. T. Wallenberger, R. Naslain, and E. I. Givergizov. Chapman and Hall, to be published.
7. T. Mah, N. L. Hecht, D. E. McCullum, J. R. Hoenigman, H. M. Kim, A. P. Katz, and H. A. Lipsitt, "Thermal Stability of SiC Fibres (Nicalon)," J. Mater. Sci., 19, 1191-201 (1984).
8. T. J. Clark, R. M. Arons, J. B. Stamatoff, and J. Rabe, "Thermal Degradation of Nicalon SiC Fibers," Ceram. Eng. Sci. Proc., 6, 576-88 (1985).
9. T. J. Clark, M. Jaffe, J. Rabe, and N. R. Langley, "Thermal Stability Characterization of SiC Ceramic Fibers: I, Mechanical Property and Chemical Structure Effects," Ceram. Eng. Sci. Proc., 7, 901-13 (1988).
10. L. C. Sawyer, R. T. Chen, F. Haimback IV, P. J. Harget, E. R. Prack, and M. Jaffe, "Thermal Stability Characterization of SiC-Ceramic Fibers: II, Fractography Structure," Ceram. Eng. Sci. Proc., 7, 914-29 (1986).
11. E. Bouillon, D. Mocaer, J. F. Villeneuve, R. Pailler, R. Naslain, M. Monthioux, A. Oberlin, C. Guimon, and G. Pfister, "Composition-Microstructure-Property Relationships in Ceramic Monofilaments Resulting from the Pyrolysis of a Polycarbosilane Precursor at 800 to 1400°C," J. Mater. Sci., 26, 1517-30 (1991).
12. K. Okamura, M. Sato, T. Seguchi, and S. Kawanishi, "Preparation of High-Temperature Strength SiC Fiber"; pp. 209-18 in Controlled Interphases in Composite Materials. Edited by H. Ishida. Elsevier Science Publishing Co., 1990.
13. M. Sugimoto, T. Shimoo, K. Okamura, and T. Seguchi, "Reaction Mechanisms of Silicon Carbide Fiber Synthesis by Heat Treatment of Polycarbosilane Fibers Cured by Radiation: I, Evolved Gas Analysis," J. Am. Ceram. Soc., 78 [4] 1013-17 (1995).
14. M. Sugimoto, T. Shimoo, K. Okamura, and T. Seguchi, "Reaction Mechanisms of Silicon Carbide Fiber Synthesis by Heat Treatment of Polycarbosilane Fibers Cured by Radiation: II, Free Radial Reaction," J. Am. Ceram. Soc., 78 [7] 1849-52 (1995).
15. H. Ichikawa, K. Okamura, and T. Seguchi, "Oxygen-Free Ceramic Fibers from Organosilicon Precursors and E-Beam Curing," Ceram. Trans., 58, 65-74 (1995).
16. G. Chollon, R. Pailler, R. Naslain, P. Olry, "Structure, Composition and Mechanical Behavior at High Temperature of the Oxygen-Free Hi-Nicalon Fiber," Ceram. Trans., 58, 299-304 (1995).
17. G. Chollon, R. Bodet, R. Pailler, and X. Bourrât, "Structure and Thermal Evolution of SiC-Based Fibers with Low Oxygen Content," Ceram. Trans., 58, 305-10 (1995).
18. J. Lipowitz, T. Barnard, D. Bujalski, J. Rab, G. Zank, A. Zangvil, and Y. Xu, "Fine-Diameter Polycrystalline SiC Fibers," Compos. Sci. Technol., 51, 167-71 (1994).
19. M. Sacks, G. W. Scheiffele, M. Saleem, G. A. Staab, A. A. Morrone, and T. J. Williams, "Polymer-Derived Silicon Carbide Fibers with Near Stoichiometric Composition and Low Oxygen Content," Mater. Res. Soc. Symp. Proc., 365, 3-10 (1995).
20. M. D. Sacks, A. A. Morrone, G. W. Scheiffele, and M. Saleem, "Characterization of Polymer-Derived Silicon Carbide Fibers with Low Oxygen Content, Near-Stoichiometric Composition and Improved Thermomechanical Stability," Ceram. Eng. Sci. Proc., 16 [4] 25-35 (1995).
21. A. Tazi-Hemida, R. Pailler, R. Naslain, J. P. Pillot, M. Birot, and J. Dunogues, "SiC-Based Fibers with Low Free Carbon Content," Ceram. Trans., 58, 311-16 (1995).
22. F. Frechette, B. Dover, V. Venkateswaran, and J. Kim, "High Temperature Continuous Sintered SiC Fiber for Composite Applications," Ceram. Eng. Sci. Proc., 12 [7] 992-1006 (1991).
23. G. V. Srinivasan and V. Venkateswaran, "Tensile Strength Evaluation of Polycrystalline SiC Fibers," Ceram. Eng. Sci. Proc., 12 [7-8] 563-72 (1993).
24. L. A. Giannuzzi, K. L. Rugg, and R. E. Tressler, "High Temperature Strength and Creep Behavior of Carborundum Alpha Silicon Carbide Fibers," Ceram. Trans., 38, 655-66 (1993).
25. R. E. Tressler and J. A. Di Carlo, "Creep and Rupture of Advanced Ceramic Fiber Reinforcements," Ceram. Trans., 57, 141-55 (1995).
26. R. S. Storm, "Recent Developments in Silicon Carbide Technology at the Carborundum Company"; pp. 51-56 in Proceedings of the 1st International Symposium on the Science and Engineering of Ceramics. Edited by S. Kimura and K. Niihara. Ceramic Society of Japan, 1991.
27. H. Tenailleau, "Characterisation des Fibres Ceramiques Si-C-N-O par Microscopie Electronique en Transmission Filtree en Energie"; Thesis No. 93-22. University of Lyon, Lyon, France, 1993.
28. N. Mozdzierz, "Relation Entre le Comportement a Haute Temperature et l'Evolution Microstructurale de Materiaux Dercmiques a Base de Carbure de Silicium"; Ph.D. Thesis. University of Paris VI, Orsay, France, 1994.
29. H. Tenailleau, "Etude de l'Oxydation de Composites a Matrice Ceramique par Microscopic TEM et Spectroscopie EELS," Internal Report No. 95-1HT, Laboratoire des Composites Thermostructuraux, France, 1995.
30. H. Tenailleau, "Etude de l'Oxydation de Composites a Matrice Ceramique par Microscopie TEM et Spectroscopie EELS," Internal Report No. 95-2HT, Laboratoire des Composites Thermostructuraux, France, 1995.
31. F. J. Frechette, W. D. G. Broecker, C. H. McMurtry, and M. R. Kasprzyk, "Non-oxide Sintered Ceramic Fibers," U.S. Pat. No. 4 908 340, March 13, 1990.
32. A. Tazi-Hemida, H. Tenaileau, L. Bardeau, R. Pailler, M. Birot, J. P. Pillot, and J. Dunogues, "Quasi-Stoichiometric SiC-Based Experimental Fibre Obtained from a Boron-Doped Polycarbosilane Precursor," unpublished work.
33. G. V. Srinivasan, V. Venkateswaran, and S. K. Lau, "An Engineering Analysis for CMC Material Design Considerations Using Carborundum's Sintered SiC Fiber and Slurry Cast/Melt Infiltration Process," Ceram. Eng. Sci. Proc., 16 [4] 63-72 (1995).
34. A. R. Venna and R. Krishna, Polymorphism and Polytropism in Crystals; p. 110. Wiley, New York, 1966.
35. S. Schamm, A. Mazel, D. Dorignac, and J. Sevely, "Observation en Microscopie Electronique a Haute Resolution du Polytypisme de SiC dans la Matrice d'un Composite SiC/SiC"; pp. 207-19 in Materiaux Composites pour Applications a Haute Temperatures; Edited by R. Naslain, J. Lamalle, and J. L. Zulian. AMAC/CODEMAC, Paris/Bordeaux, France, 1990.