3He NMR of HeΓ606- and HeΓ706-. New records for the most shielded and the most deshielded 3He inside a fullerene

Journal of the American Chemical Society

Volumn 120, Issue 25, 1998, Pages 6389-6393

  Shabtai, Elad ^a   Weitz, Amir ^a   Haddon, Robert C ^b   Hoffman, Roy E ^a   Rabinovitz, Mordecai ^a   Khong, Anthony ^c   Cross, R James ^c   Saunders, Martin ^c   Cheng, Pei Chao ^d   Scott, Lawrence T ^d  

^a HEBREW UNIVERSITY OF JERUSALEM   (Israel)

^b UNIVERSITY OF KENTUCKY   (United States)

^c YALE UNIVERSITY   (United States)

^d BOSTON COLLEGE   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

FULLERENE; LITHIUM;

ARTICLE; ELECTRON MICROSCOPY; ELECTRON SPIN RESONANCE; ENVIRONMENTAL TEMPERATURE; MAGNETISM; NUCLEAR MAGNETIC RESONANCE; PREDICTION; ULTRASOUND;

EID: 0032127481     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja9805831     Document Type: Article

References (45)

1. Presented at the Fifth Chemical Congress of North America, November 11-15, 1997, Cancun, Mexico, abstract No. 1785.
2. Minkin, V. I.; Glukhovtsev, M. N.; Simkin, B. Y. Aromaticity and Antiaromaticity; Wiley: New York, 1994.
3. Haddon, R. C. J. Am. Chem. Soc. 1978, 100, 1722-1728.
4. Haddon, R. C. Science 1993, 261, 1545-1550.
5. Pasquarello, M.; Schluter, M.; Haddon, R. C. Science 1992, 257, 1660-1661.
6. Fowler, P. W. Chem. Phys. Lett. 1995, 238, 270-280.
7. Suzuki, T.; Li, Q.; Khemani, K. C.; Wudl, F. J. Am. Chem. Soc. 1992, 114, 7301-7302.
8. Haddon, R. C.; Pasquarello, A. Phys. Rev. B 1994, 50, 16459-16463.
9. Haddon, R. C; Schneemeyer. L. F.; Waszczak, J. V.; Glarum, S. H.; Tycko, R.; Dabbagh, G.; Kortan, A. R.; Muller, A. J.; Mujsce. A. M.; Rosseinsky, M. J.; Zahurak, S. M.; Makhija, A. V.; Thiel, F. A.; Raghavachari, K.; Cockayne, E.; Elser, V. Nature 1991, 350, 46-47.
10. Ruoff, R. S.; Beach, D.; Cuomo, J.; McGuire, T.; Whetten, R. L.; Diederich, F. J. Phys. Chem. 1991, 95, 3457-3459.
11. Saunders, M.; Jimenez-Vazquez, H. A.; Cross, R. J.; Mroczkowski, S.; Freedberg, D. I.; Anet, F. A. L. Nature 1994, 367, 256-258.
12. Haddon, R. C. Nature 1995, 378, 249-255.
13. (a) Rabinovitz, M.; Willner, I.; Minsky, A. Acc. Chem. Res. 1983, 16, 298-304.
14. (b) Müllen, K. Chem. Rev. 1984, 84, 603-46.
15. (c) Rabinovitz, M.; Cohen, Y. Adv. Chem. Ser 1988, 217, 53-72.
16. (d) Rabinovitz, M.; Ayalon, A. Pure Appl. Chem. 1993, 65, 111-18.
17. Pasquarello, M.; Schluter, M.; Haddon, R. C. Phys. Rev. A 1993, 47, 1783-1789.
18. Elser, V.; Haddon, R. C. Nature 1987, 325, 792-794.
19. Bühl, M.; Thiel, W.; Jiao, H.; Schleyer, P. v. R.; Saunders, M.; Anet, F. A. L. J. Am. Chem. Soc. 1994, 116, 6005-6006.
20. Diederich, J.; Gangopadhyay, A. K.; Schilling, J. S. Phys. Rev. B 1996, 54, 9662-9665.
21. Bühl, M.; Thiel, W. Chem. Phys. Lett. 1995, 233, 585-589.
22. Cioslowski, J. Chem. Phys. Lett. 1994, 227, 361-364.
23. Bühl, M. Chem. Euro. J. 1998, 4, 734-739.
24. Saunders, M.; Jimenez-Vazquez, H. A.; Cross, R. J.; Billups, W. E.; Gesenberg, C.; Gonzalez, A.; Luo, W.; Haddon, R. C.; Diederich, F.; Herrmann, A. J. Am. Chem. Soc. 1995, 117, 9305-9308.
25. Xie, Q.; Perez-Cordero, E.; Echegoyen, L. J. Am. Chem. Soc. 1992, 114, 3978-80.
26. (a) Haddon, R. C.; Brus, L. E.; Raghavachari, K. Chem. Phys. Lett. 1986, 125, 459-64.
27. (b) Disch, R. L.; Schulman, J. M. Chem. Phys. Lett. 1986, 125, 465-6.
28. (c) Fowler, P. W.; Woolrich, J. Chem. Phys. Lett. 1986, 127, 78-83.
29. Haddon, R. C. Acc. Chem. Res 1992, 25, 127-131.
30. Bausch, J. W.; Prakash, G. K. S.; Olah, G. A.; Tse, D. S.; Lorents, D. C.; Bae, Y. K.; Malhotra, R. J. Am. Chem. Soc. 1991, 113, 3205-6.
31. Saunders, M.; Anet, F. A. L.; Prakash, S. Unpublished results2E
32. Weitz, A. Ph.D. dissertation, The Hebrew University, Jerusalem, Israel, 1996.
33. (a) Ayalon, A.; Sygula, A.; Cheng, P.-C.; Rabinovitz, M.; Rabideau, P.; Scott, L. T. Science 1994, 265, 1065-1067.
34. (b) Ayalon, A.; Rabinovitz, M.; Cheng, P. C.; Scott, L. T. Angew. Chem. 1992, 104, 1691-2 (see also: Angew. Chem., Int. Ed. Engl. 1992, 31, 1636-7).
35. (b) Ayalon, A.; Rabinovitz, M.; Cheng, P. C.; Scott, L. T. Angew. Chem. 1992, 104, 1691-2 (see also: Angew. Chem., Int. Ed. Engl. 1992, 31, 1636-7).
36. (c) Ayalon, A. Ph.D. Dissertation, The Hebrew University, Jerusalem, Israel, 1994.
37. 70 to their anions without sonication, although they both appear to function less efficiently than corannulene, i.e., the reductions mediated by these planar polycyclic aromatic hydrocarbons gave lower yields of the fullerene anions (weaker spectra) even after several days.
38. Baumgarten, M.; Gherghel, L.; Wagner, M.; Weitz, A.; Rabinovitz, M.; Cheng, P.-C.; Scott, L. T. J. Am. Chem. Soc. 1995, 117, 6254-7.
39. 70 species that is even more highly reduced than the hexaanion.
40. (a) Homer, J.; Beevers, M. S. J. Magn. Reson. 1985, 63, 287-97.
41. (b) Homer, J.; Roberts, J. K. J. Magn. Reson. 1987, 74, 424.
42. (c) Hoffman, R. E.; Davies, D. B. J. Magn. Reson. 1988, 80, 318-23.
43. Nir, M.; Shapiro, I. O.; Hoffman, R. E.; Rabinovitz, M. J. Chem. Soc., Perkin Trans. 2 1996, 1607-1616.
44. (a) Van Geet, A. L. Anal. Chem. 1968, 40, 2227-9.
45. (b) Van Geet, A. L. Anal. Chem. 1970, 42, 679-80.