Determination of eight trichothecenes by gas chromatography-mass spectrometry after sample clean-up by a two-stage solid-phase extraction

Journal of Chromatography A

Volumn 815, Issue 1, 1998, Pages 123-132

  Schollenberger, M ^a   Lauber, U ^a   Terry Jara, H ^a   Suchy, S ^a   Drochner, W ^a   Muller H M ^a  

^a UNIVERSITY OF HOHENHEIM   (Germany)

Author keywords

Food analysis; Mycotoxins; Sample handling; Trichothecenes

Indexed keywords

MYCOTOXIN; TRICHOTHECENE DERIVATIVE;

ARTICLE; CEREAL; DERIVATIZATION; EXTRACTION; FECES; FOOD ANALYSIS; FUSARIUM; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; MOULD; NONHUMAN; PRIORITY JOURNAL; SAMPLE; SOLID PHASE EXTRACTION; SWINE; TOXIN ANALYSIS;

ANIMALS; BREAD; FECES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; INDICATORS AND REAGENTS; MYCOTOXINS; ORYZA SATIVA; SWINE; TRICHOTHECENES; TRITICUM;

EID: 0031828374     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0021-9673(98)00454-3     Document Type: Article

References (33)

1. Y. Ueno (Ed.), Trichothecenes-Chemical, Biological and Toxicological Aspects, Elsevier, Amsterdam, New York, 1983.
2. W.F.O. Marasas, P.E. Nelson, T.A. Tousson, Toxigenic Fusarium species-Identity and Mycotoxicology, Pennsylvania State University Press, University Park, London, 1984.
3. W.F.O. Marasas, in: J.E. Smith, R.S. Henderson (Eds.), Mycotoxins and Animal Foods, CRC Press, Boca Raton, FL, 1991, p. 119.
4. M. Gareis, J. Bauer, J. Enders, B. Gedek, in: J. Chelkowski (Ed.), Fusarium Mycotoxins-Taxonomy and Pathogenicity, Elsevier, Amsterdam, New York, 1989, p. 441.
5. P.M. Scott, in: V.R. Beasley (Ed.) Trichothecene Mycotoxicosis: Pathophysiologic Effects, CRC Press, Boca Raton, FL, 1989, p. 1.
6. Scott P.M. Food Add. Contam. 14:1997;339.
7. Müller H.-M., Reimann J., Schumacher U., Schwadorf K. Natural Toxins. 5:1997;24.
8. Müller H.-M., Reimann J., Schumacher U., Schwadorf K. Mycopathologia. 137:1997;185.
9. H.-M. Müller, J. Reimann, U. Schumacher, K. Schwadorf, Food Add. Contam. (1998) in press.
10. Kuiper-Goodman T., Scott P.M., Watanabe H. Regulat. Toxicol. Pharmacol. 7:1987;253.
11. B. Francis, in: V.R. Beasley (Ed.), Trichothecene Mycotoxicosis: Pathophysiologic Effects. Vol. I, CRC Press, Boca Raton, FL, p. 107.
12. R.D. Wyatt, in: J.E. Smith, R.S. Henderson (Eds.), Mycotoxins and Animal Foods, CRC Press, Boca Raton, FL, 1991, p. 553.
13. Rotter B.A., Prelusky D.B., Pestka J.J. J. Toxicol. Environ. Health. 48:1996;1.
14. Gilbert J. Food Add. Contam. 10:1993;37.
15. Scott P.M. Food Add. Contam. 12:1995;395.
16. Gilbert J., Boenke A., Wagstaffe P.J. Food Add. Contam. 9:1992;71.
17. Tacke B.K., Casper H.H. J. AOAC Int. 79:1996;472.
18. Gareis M., Bauer J., Gedek B. Tierärztl. Praxis Suppl. 1:1985;8.
19. Scott P.M. J. Assoc. Off. Anal. Chem. 69:1986;889.
20. Sydenham E.W., Thiel P.G. Food Add. Contam. 4:1987;472.
21. Romer T.R. J. AOAC Int. 69:1985;699.
22. Croteau S.M., Prelusky D.B., Trenholm H.L. J. Agric. Food. Chem. 42:1994;928.
23. Wegmüller F., Steiner W. Mitt. Gebiete Lebensm. Hyg. 85:1994;553.
24. Furlong E.B., Soares L.M.V. J. AOAC Int. 78:1995;386.
25. Tanaka T., Hasegawa A., Matsuki Y., Ishii K., Ueno Y. Food Add. Contam. 2:1985;125.
26. Kientz C.E., Verwej A. J. Chromatogr. 355:1986;229.
27. Schwadorf K., Müller H.-M. Chromatographia. 32:1991;137.
28. A.G. Harrison, Chemical Ionisation Mass Spectrometry, CRC Press, Boca Raton, FL, 1983, p. 31.
29. H.J. Hübschmann, Chemische Ionisierung an Ion-Trap-Massenspektrometern, Firmenschrift der Axel Semrau GmbH, Sprockhövel, 1993, p. 12.
30. Seidel V., Lang B., Fraißler S., Lang C., Schiller K., Filek G., Lindner W. Chromatographia. 37:1993;191.
31. DIN 32 645, Deutsche Norm, Nachweis-, Erfassungs- und Bestimmungsgrenze, ICS 71.040.40, Stand 5/94.
32. Bergsjö B., Matre T., Nafstad I. J. Vet. Med., Ser. A. 39:1992;752.
33. Scott P.M., Kanhere S.R., Tarter E. J. Assoc. Off. Anal. Chem. 69:1986;889.